Shale in the Jurassic Lianggaoshan Formation in central Sichuan exhibits strong heterogeneity. The study of the pore structure characteristics of different lithologies is crucial to the selection of the target interval. Shale samples of the Lianggaoshan Formation from well YS5 in the central part of the Sichuan Basin were analyzed using scanning electron microscopy, low-temperature nitrogen adsorption, high-pressure mercury injection (HPMI), and large -field splicing method -based scanning electron microscopy (LFS-SEM) to elucidate the pore structure characteristics of shale and their influencing factors. The mineral composition of the reservoir in the study area was diverse, primarily consisting of clay minerals, followed by quartz and calcite. The reservoir space comprised intergranular, granular, and organic matter pores, and oil was observed to fill the reservoir space. Reservoir characteristics varied with the lithological properties. In clayey shale, intergranular pores located in clay mineral particles and pores between pyrite and natural fractures were mainly observed, with a bimodal distribution of pore size and peak distribution of 10–50 nm and >100 nm. The storage space of ash-bearing shale mainly consisted of intragranular pores and intergranular (crystalline) micropores, with pore sizes primarily concentrated in the 10–50 nm range. The storage space in silty shale mainly developed in clastic mineral particles such as quartz, followed by clay mineral intergranular pores with a relatively wide distribution of sizes. Pores were mainly inkbottle-shaped and slit-type/plate-type pores, with an average specific surface area of approximately 6.9046 m2·g−1 and an average pore volume of approximately 0.0150 cm3·g−1. The full-pore capillary pressure curve was established using a combination of gas adsorption–desorption tests and HPMI. The fractal dimension of the sample pore structure was calculated, and a significant linear correlation was found between clay mineral content and the fractal dimension. Thus, the pore structure characteristics were mainly controlled by the content and distribution of clay minerals.
Natural fractures are of paramount importance in storing carbon in shale oil reservoirs, where ultra-low porosity and permeability necessitate their essentiality for enhanced oil recovery. Therefore, comprehensively clarifying the characteristics of natural fractures in shale oil reservoirs is imperative. This paper focuses on investigating the microscopic features of natural fractures in organic-rich continental shale oil reservoirs that are commonly found in the Lower Jurassic strata of the Sichuan Basin, employing them as a representative example. Multiple methods were utilized, including mechanical testing, Kaiser testing, multi-scale CT scanning (at 2 mm, 25 mm, and 100 mm scales), and a numerical simulation of fluid seepage in fracture models. The results revealed that the in situ stress of the target seam displays the characteristic of σH > σv > σh, with σv and σh being particularly similar. The relatively high lateral stress coefficient (ranging from 1.020 to 1.037) indicates that the horizontal stresses are higher than the average level. Although the 2 mm CT scan provides a more detailed view of fractures and connected pores, it primarily exhibited more pore information due to the high resolution, which may not fully unveil additional information about the fractures. Thus, the 25 mm shale core is a better option for studying natural fractures. The tortuosity of the different fractures indicated that the morphology of larger fractures is more likely to remain stable, while small-scale fractures tend to exhibit diverse shapes. The simulations demonstrated that the stress sensitivity of fracture permeability is approximately comparable across different fracture scales. Therefore, our research can enhance the understanding of the properties of natural fractures, facilitate predicting favorable areas for shale oil exploration, and aid in evaluating the carbon storage potential of shale oil reservoirs.
Thermal maturity of the shales from the Ziliujing Formation of the Jurassic age in the Sichuan Basin is in the hydrocarbon generation window, which makes it a candidate for shale oil and gas development. The meso- and macropore characteristics and heterogeneity of shales are important factors affecting the occurrence and development of oil and gas. However, the meso- and macropores of the Ziliujing shales have not been systematically studied. Thus, the mineral compositions and total organic carbon (TOC) of samples from this formation, as well as its pore structure, are analyzed by low-temperature N2 adsorption technique. Moreover, the heterogeneity of the pores was determined by multifractal analysis. The results show that the Ziliujing shales can be classified into three types according to the distributions of mineral compositions of carbonate and mixed and argillaceous shales. Results revealed that the smallest meso- and macropore volume (PV), the smallest specific surface area (SSA), and the largest average pore diameter (APD) occur in the carbonate shales. However, the largest PV and SSA and the smallest APD are observed in the argillaceous shales. The porosity of carbonate shales is mainly concentrated between 5 nm and 30 nm. Compared with carbonate shales, the porosity with pore sizes less than 30 nm of mixed and argillaceous shales shows a rapid increase. Furthermore, inorganic minerals are the main factors affecting the pore distributions, while TOC shows a weak effect. Herein, clay minerals significantly increase the mesopore volume and the pore number with a size of less than 30 nm. The Dq-q curves reveal that the meso- and macropore distributions of Ziliujing shales show multifractal behavior, but the multifractal characteristics of pores of various shales are distinctly different. The information dimension D1, the Hurst exponent H, and the width of the right side D0–D10 are key indicators to distinguish the local variations within the pore structure of different types of shales. The carbonate shales have the largest multifractal spectra width and the smallest D1 and H, while the opposite trend is found for the argillaceous shales. Clay minerals reduce the heterogeneity of the meso- and macropore distributions and increase the pore connectivity. Nevertheless, the carbonate minerals exhibit a reverse trend. Finally, it was found that TOC does not impact pore complexity as much. Collectively, this study supports our understanding of the occurrence of shale oil within various reservoir facies, thereby providing a guideline for future explorations in the Ziliujing Formation of the Jurassic age in the Sichuan Basin.
The features and formation stages of natural fractures have significant influences on the fracturing of shale reservoirs and the accumulation of oil and gas. The characteristics and evolution of tectonic fractures in the Lianggaoshan Formation in Northeast Sichuan were investigated based on outcrops, drill cores, geochemical data, and acoustic emission test results. Our results demonstrated that the fracture types of the Lianggaoshan Formation were mainly low-degree bedding-slip fractures, followed by high-degree through-strata shear fractures and vertical tensile fractures. The influences of strike-slip faults on the fractures were stronger than those of thrust faults; fractures in thrust faults were concentrated in the hanging wall. The densities of tensile and shear fractures were inversely proportional to the formation thickness, while the density of interlayer slip fractures was independent of the formation thickness. The density of tectonic fractures was proportional to the quartz content. The fractures of the Lianggaoshan Formation were generated in three stages during uplift: (1) Late Yanshan–Early Himalayan tectonic movement (72~55 Ma), (2) Middle Himalayan tectonic movement (48~32 Ma), (3) Late Himalayan tectonic movement (15 Ma~4 Ma). Fractures greatly improve the oil and gas storage capacity and increase the contents of free and total hydrocarbons. At the same time, they also reduce the breakdown pressure of strata. This study facilitated the prediction of the fracture distribution and oil and gas reservoirs in the Lianggaoshan Formation and provided references for the selection of favourable areas for shale oil and the evaluation of desert sections in the study area.
1 June 2021 in IOP Conference Series: Earth and Environmental Science
The enrichment law of desserts in Xujiahe formation of Sichuan Basin has become the core problem of tight sandstone gas reservoir. In view of this problem, taking the member 2 of Xujiahe Formation in Yingshan area of Sichuan Basin as an example, the author analyzes the main factors of enrichment of natural gas through the analysis of the basic geological features of sedimentary environment, reservoir, hydrocarbon source, structure and reservoir formation, and then discusses enrichment mode of natural gas. The results show that the reservoir forming conditions of member 2 in Yingshan area are superior, and the widely covered source rocks are developed, and the source rocks have good hydrocarbon generation potential. The sand bodies in the delta front with thick layers are deposited in member 2 of Xujiahe, which is distributed in large area, which lays the foundation for the development of high-quality reservoirs. The reservoir space types are various, mainly mainly including primary intergranular pores, dissolution pores and micro fractures, and the reservoir has good physical properties. The accumulation of natural gas in Yingshan structure is the result of coupling of the following factors: the development of high-quality reservoir controls the distribution of natural gas; the structural background is conducive to the enrichment of natural gas; the good matching relationship between faults and traps controls the differential accumulation of natural gas in the reservoir.