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In this paper, we report the use of magnesium alloy (AZ31B) as the matching material for PZT-5H ultrasonic transducers. The AZ31B has an acoustic impedance of 10.3 MRayl, which provides a good acoustic impedance match for PZT-5H ultrasonic transducers in water medium based on the double matching layer theory. Two PZT-5H transducers with different center frequencies were designed and fabricated using the AZ31B. The respective center frequencies of the two fabricated transducers were 4.6 MHz and 9.25 MHz. The 4.6 MHz transducer exhibits a −6 dB bandwidth of 79% and two-way insertion loss of −11.11 dB. The 9.25 MHz transducer also shows good performance: −6 dB bandwidth of 71% and two-way insertion loss of −14.43 dB. The properties of the two transducers are superior to those of transducers using a composite matching layer, indicating that the magnesium alloy may be a promising alternative for high-performance transducers.