In this paper, the preparation and characterisation of polymer materials suitable for single point incremental forming (SPIF) technology were performed. Three different kinds of mixtures were selected: a mixture of neat polyamide 12 (PA12), a nanocomposite with PA12 matrix and 1% clay (Cloisite 93A), and a nanocomposite with PA12 matrix and 3% clay (Cloisite 93A). Materials were produced using a melt intercalation method followed by compression moulding. According to the needs of SPIF technology, morphological and mechanical properties were investigated in the obtained mixtures. Transmission electron microscopy (TEM) and X-ray diffraction (XRD) were used to characterize morphological properties. It was determined that the most desired obtained exfoliated structure of clay in the polymer matrix was achieved. Static tensile testing and dynamic mechanical analysis as well as the determination of glass transition temperature and crystallinity of all analysed materials were used to obtain mechanical and thermal properties of the mixtures. The results obtained for each mixture were compared with respect to the content of clay. The content of clay (Cloisite 93A) showed a strong influence on the properties of the obtained materials. The presence of clay (Cloisite 93A) affected the increase of tensile strength and Young’s modulus, while its influence on the attained elongation was not unique.
18 September 2018 in Materials Performance and Characterization
The purpose of this research is to upgrade the mathematical modeling and computer simulation of steel quenching. Based on theoretical analyses of physical processes that exist in quenching systems, the mathematical model for steel quenching is established and computer software is developed. The mathematical model of steel quenching is focused on physical phenomena, such as heat transfer, phase transformations, mechanical properties, and generation of stresses and distortions. The numerical procedure of computer simulation of steel quenching is divided into three parts: numerical calculation of transient temperature field, numerical calculation of phase change, and numerical calculation of the mechanical behaviors of steel during quenching. The numerical procedure is based on the finite volume method. Physical properties that were included in the model, such as heat conductivity coefficient, heat capacity, and surface heat transfer coefficient, were obtained by the inversion method based on the Jominy test results. By the completed algorithm, 3-D situation problems, such as the quenching of complex cylinders, cones, spheres, etc., can be simulated. The established model of steel quenching can be successfully applied in the practical usage of quenching.
10 August 2018 in IOP Conference Series: Materials Science and Engineering
Numerical model of controlled cooling in the production of steel hot rolled bars was developed. The numerical model and algorithm are completed to solve problems in controlled cooling of hot rolled bars in cooling beds. The controlled cooling is performed by special placement of hot rolled bars on cooling beds. By numerical model of controlled cooling is possible to predict a transient temperature field, microstructure evolution and hardness of round steel bars during their cooling in cooling beds. The numerical model of transient temperature field is based on control volume method. The hardness and microstructure distribution in steel bars has predicted by using equations of austenite decomposition kinetic. The algorithm for prediction is based the real chemical composition. Numerical model and computer program were experimentally verified by experimental work in a real industrial production of low-alloyed steel bars. The verification of developed numerical model was performed by comparison of simulated with experimentally evaluated results hardness and cooling curve.