Herein, the effects of height-diameter ratios (H/D) on the microstructure evolution and mechanical properties of 0.4C-Si-Mn-Cr steel during high temperature deformation are reported. The compression experiments were performed on steel samples using Gleeble to obtain a reasonable deformation temperature, and the degree of deformation was assessed in the range of 1.5 to 2.0 H/D via forging. The forged specimens were quenched using the same heat treatment process. The hardness and impact toughness of the steel samples were tested before and after heat treatment. Grain sizes gradually increased with an increase in the compression temperature from 950 °C to 1150 °C, and the grain sizes decreased with an increase in H/D. The microstructure of the steel samples contained pearlite, bainite, martensite, and retained austenite phase. The microstructure after forging was more uniform and finer as compared to that of as-cast steel samples. The hardness and impact toughness of the steel samples were evaluated after forging; hardness first increased and then decreased with an increase in H/D, while the impact toughness continuously increased with an increase in H/D. Hence, the microstructure and properties of steel could be improved via high temperature deformation, and this was primarily related to grain refinement.
20 May 2023 in Journal of Materials Research and Technology
In this paper, WC particles reinforced steel matrix composites (WCP/SMC) doped with rare-earth elements Y, Ce, La, and Nd, are manufactured via powder metallurgy sintering. The interface and mechanical properties of WCP/SMC are theoretically and experimentally investigated. The microstructures are observed through SEM, EDS and XRD. The properties are determined by compression and micro-hardness tests. The effects of rare-earth element doping on interface and mechanical properties of composites are investigated. The results indicate that composites mainly consist of α-Fe, W2C, WC, and Fe3W3C. In addition, the doping can accelerate the inter-atomic diffusion of the atoms in the interfacial reaction zone, promote the formation of Fe3W3C phase, and widen the interfacial reaction zone. Doping of rare-earth elements can reduce the hardness difference between the interfacial reaction zone and the composite matrix from 10.15 to 5.71 GPa and increases the compressive strength from 296.7 to 659.2 MPa. First-principles calculations indicate that doping of rare earth can reduce the interfacial, formation, and dissolution energy between the WC particles and the iron matrix. Thus, the stability of the interfacial reaction zone and bonding between the WC particles and the matrix is improved. By comparing the results with first-principles based calculations, composites doped with Nd have the best relative reaction interface bonding and mechanical properties.
Alloyed high manganese steel is a general type of wear-resistant steel, and its precipitates and austenite matrix grain sizes play an important role in impact abrasive wear behavior. Solid-solution treatment is an effective method to balance the size of the austenite grains and precipitates. This work attempts to find a new progressive solid-solution treatment to make alloyed high manganese steel castings refine the microstructure and balance the wear resistance under impact abrasive wear conditions. Compared with traditional solid-solution treatment, the MC- and M23C6-type carbide precipitates resulting from progressive solid-solution treatment decrease, and the tensile strength and impact toughness of steel are significantly increased. After the solid-solution treatment at different heating rates, the grain refinement effect is remarkable after shortening the holding time at 1100 °C and increasing the heating rate to 150 °C h−1. The impact abrasive wear test results show that, compared with the traditional solid-solution treatment at 1100 °C for 4 h, the wear resistance of high manganese steel has a 23.1% improvement after progressive solution treatment at 1100 °C for 2 h, and the wear failure forms of all the experimental steels are microcutting, oxidation wear and plastic deformation.