Disposable electrochemically reduced graphene oxide-based (ERGO) screen-printed electrodes (SPE) were developed for the determination of total tetracyclines as a sample screening approach. To this end, a selective adsorption-detection approach relied on adsorptive transfer stripping differential pulse voltammetry (AdTDPV) was devised, where the high adsorption capacity and the electrochemical properties of ERGO were simultaneously exploited. The approach was very simple, fast (6 min.), highly selective by combining the adsorptive and the electrochemical features of tetracyclines, and it used just 10 μL of the sample. The electrochemical sensor applicability was demonstrated in the analysis of environmental and food samples. The not-fully explored AdTDPV analytical possibilities on disposable nanostructured transducers become a new tool in food and environmental fields; drawing new horizons for “in-situ” analysis.

• The use of ultrasound in the South Cone Region is highlighted. • South Cone comprises Argentina, Chile, Southern Brazil and Uruguay. • This review presents the uses of ultrasonic energy in synthesis (organic and inorganic). • The application of ultrasound energy in analytical methods is presented.

A new, inexpensive and easy to use 3D printable device was developed for nephelometric and fluorimetric determination. Its applicability was tested for the quantification of quinine in tonic drinks and sulfate in natural water with good analytical accuracy. In this way, sulfate determination was carried out by nephelometry using a red LED, while quinine was determined using a blue LED by fluorimetry. A smartphone camera was used to take the pictures and afterwards transform them into the RGB color space using the software ImageJ by a personal computer. The linear range was 2.0–50.0 mg L⁻¹ for sulfate with a LOD of 0.13 mg L⁻¹, and the corresponding quantification limit (LOQ) was 0.43 mg L⁻¹. The linear range for quinine was from 0.42 to 3.10 mg L⁻¹. The LOD and LOQ were 0.11 mg L⁻¹ and 0.38 mg L⁻¹, respectively.