The electrochemical reduction of cinnarizine was investigated by cyclic and linear sweep adsorptive voltammetry at glassy carbon electrode in Britton-Robinson buffers over the pH range 2.5–11.5. For analytical purposes, a well-defined adsorption-controlled cathodic peak was obtained at pH 2.5. By cathodic adsorptive linear sweep voltammetry, a linear calibration plot was obtained in the range of 2.0 × 10⁻⁷ to 5.0 × 10⁻⁶ mol L⁻¹ with detection limit of 9.0 × 10⁻⁹ mol L⁻¹. The method was successfully applied to the determination of cinnarizine in commercial formulations with mean recovery and relative standard deviation of 100.24% and 1.46, respectively. The proposed method was also applied for drug determination in spiked serum samples by applying the standard addition method with a mean recovery of 97.80% and standard deviation of 3.06.

The electrochemical reduction of secnidazole was carried out in BR buffer solutions in the pH range 2.0–11.8 by dc polarography. The polarograms exhibited two irreversible reduction waves in acidic media and one wave in alkaline media, corresponding to the reduction of nitro group in the drug. The cathodic adsorptive voltammetric behavior was studied on glassy carbon electrode to optimize an analytical method for determination of secnidazole. The drug was determined in the range between 4.0×10−6 and 1.2×10−4molL−1. The proposed method was successfully applied to the determination of the drug content in tablets with mean recovery and relative standard deviation of 100.91% and 1.82%, respectively. It was also applied to human serum with a good precision and accuracy

In wireless sensor/ad hoc networks, all wireless nodes frequently flood the network channel by transmitting control messages causing “broadcast storm problem”. Thus, inspired by the physical backbone in wired networks, a Virtual Backbone (VB) in wireless sensor/ad hoc networks can help achieve efficient broadcasting. A well-known and well-researched approach for constructing virtual backbone is solving the Connected Dominating Set (CDS) problem. Furthermore, minimizing the size of the CDS is a significant research issue. We propose a new parallel scatter search algorithm with elite and featured cores for constructing a wireless sensor/ad hoc network virtual backbones based on finding minimum connected dominating sets of wireless nodes. Also, we addressed the problem of VB node/nodes failure by either deploying a previously computed VBs provided by the main pSSEF algorithm that does not contain the failed node/nodes, or by using our proposed FT-pSSEF algorithm repairing the broken VBs. Finally, as nodes in a VB incur extra load of communication and computation, this leads to faster power consumption compared to other nodes in the network. Consequently, we propose the virtual backbone scheduling algorithm SC-pSSEF which aims to find multiple VBs using the VBs provided by the pSSEF algorithm and switch between them periodically to prolong the network life time.

Sugarcane stalks powder was tested for its efficiency of removing a textile dye Maxilon Red GRL from aqueous solution. Different parameters affecting dye removal efficiency were studied. These parameters include contact time, initial dye concentration, adsorbent dose, ionic strength, pH, and temperature. Langmuir and Freundlich isotherm models were applied to the equilibrium data. The data fitted well with the Langmuir isotherm (). The maximum monolayer adsorption capacity () was found to be 20.96 mg/g at an initial pH of 7.2. The temperature variation study showed that dye adsorption is exothermic and spontaneous with increased randomness at the solid solution interface. The results indicated that sugarcane stalks could be an alternative for more costly adsorbents used for dye removal. The kinetic of the adsorption process followed the pseudo second-order kinetics model.