NM550 wear-resistant steel is widely used in large-scale engineering and mining machinery under extremely harsh working conditions. In NM550 steel, the addition of Ti can cause the formation of micron-scale TiN and TiC inclusions, easily triggering cleavage fractures. The fracture behavior and precipitation rule of micron-scale TiN and TiC inclusions on the tensile process in NM550 steel was investigated by scanning electron microscopy, transmission electron microscopy, and energy spectrum analysis combined with thermodynamic theory. The TiN precipitated in the solid–liquid two-phase region at a precipitation temperature of 1710 K, whereas that of TiC was 1158 K along the austenite grain boundary. The sizes of the TiN precipitated in the liquid phase and the TiC precipitated in austenite were both at the micron scale, which is prone to cleavage fracture during the stretching process. Under tensile stress, microcracks were first initiated at the TiN inclusion, which were further separated forming a hole, whereas the TiC inclusion was divided into two sections with a long and narrow gap formed between the substrates. The sizes of the TiN and TiC were related to the cooling rate, Ti, and N contents. The larger the cooling rate and the lesser the Ti and N content, the smaller the TiN and TiC sizes.
12 October 2022 in Animal Models and Experimental Medicine
Background: Flight and freezing are two vital defensive behaviors that mice display to avoid natural enemies. When they are exposed to innate threats, visual cues are processed and transmitted by the visual system into the emotional nuclei and finally transmitted to the periaqueductal gray (PAG) to induce defensive behaviors. However, how the dorsal PAG (dPAG) encodes the two defensive behaviors is unclear.Methods: Multi‐array electrodes were implanted in the dPAG nuclei of C57BL/6 mice. Two kinds of visual stimuli (looming and sweeping) were used to induce defensive behaviors in mice. Neural signals under different defense behaviors were recorded, and the encoding characteristics of the two behaviors were extracted and analyzed from spike firing and frequency oscillations. Finally, synchronization of neural activity during the defense process was analyzed.Results: The neural activity between flight and freezing behaviors showed different firing patterns, and the differences in the inter‐spike interval distribution were mainly reflected in the 2–10 ms period. The frequency band activities under both defensive behaviors were concentrated in the theta band; the active frequency of flight was ~8 to 10 Hz, whereas that of freezing behavior was ~6 to 8 Hz. The network connection density under both defense behaviors was significantly higher than the period before and after defensive behavior occurred, indicating that there was a high synchronization of neural activity during the defense process.Conclusions: The dPAG nuclei of mice have different coding features between flight and freezing behaviors; during strong looming stimulation, fast neuro‐instinctive decision making is required while encountering weak sweeping stimulation, and computable planning late behavior is predicted in the early stage. The frequency band activities under both defensive behaviors were concentrated in the theta band. There was a high synchronization of neural activity during the defense process, which may be a key factor triggering different defensive behaviors.
The microstructure and mechanical properties of X70 pipeline steel with a ferrite/martensite dual-phase microstructure produced by thermo-mechanical controlled processing were investigated by tensile tests, Charpy V-notched (CVN) impact tests, drop-weight tear tests, guided-bend tests, scanning electron microscopy and transmission electron microscopy combined with thermodynamic simulation analysis. All the mechanical properties met the strength, ductility, toughness and deformability properties requirements of X70 grade pipeline steel with strain-based design. The shear fracture area and absorbed energy of CVN at −10 °C were >97% and >205 J in base metal (BM), weld metal (WM) and heat affected zone (HAZ) with low transition temperature, indicating adequate resistance to propagating fracture. The microstructure of WM was mainly intragranular acicular ferrite that can guarantee high strength, toughness and over matching requirements of the welded joint. Because of being exposed to successive heat inputs, the ferrite plus martensite/bainite microstructure of BM was heated between Ac1 and Ts forming the HAZ. However, a high CVN impact toughness of 345 J at −10 °C in HAZ was obtained, which indicated that the excellent mechanical properties of BM would not be seriously deteriorated during the welding thermal cycles with the reasonable addition of Ti and Nb.
The 5% Ni steel is often used to make steel storage tanks to store liquefied natural gas (LNG). Herein, the microstructure and mechanical properties of 5% Ni steel samples during bending were studied through combining scanning electron microscopy, energy dispersive spectroscopy, optical microscopy, X-ray diffraction, and electron backscattered diffractometer methods with tensile tests. The outer and inner arcs underwent tensile and compressive stress, respectively, resulting in a severely deformed microstructure with a high density of dislocation, improving both the tensile and yield strengths. The ductility of the 5% Ni steel samples decreased significantly after bending due to the work hardening and dislocation accumulation. During bending, the shear bands occurred at the surface or subsurface, which were caused by strain localization. Amounts of “harder” grains with high TF and more orange and red KAM areas with high local strain at the outer and inner arcs produced a greater stress concentration than that of the mid-thickness, which can induce crack initiation and propagation due to the large deformation during bending.
High-strength, wear-resistant steel often suffers from delayed cracking after flame cutting. Delayed cracking can lead to extremely harmful sudden brittle fracture; therefore, it is necessary to study the formation of delayed cracking in high-strength steel. This work investigated the influence of TiN inclusions and segregation on the delayed cracking in NM450 wear-resistant steel by optical microscopy, scanning electron microscopy, X-ray diffraction, transmission electron microscopy and electron backscattered diffractometer methods. The results indicated that the delayed cracks originated from the segregation zones (SZs) containing multiple high-hardness segregation bands. The tensile strength of the SZ specimens was higher than that of non-segregation zone (NSZ) specimens, while the total elongation and reduction of area of the SZ specimens were relatively lower compared with the NSZ specimens. Therefore, the delayed cracking on the flame cutting surface of the NM450 steel plate was attributed to the existence of SZs that contain a high density of dislocations and considerable micro-sized TiN inclusions.
This paper aims to study the relationship between the microstructure and the mechanical properties of X70 submarine pipeline steel with 40.5 mm thickness. The microstructure was examined by using optical microscopy, scanning electron microscopy and an electron backscattered diffractometer, while the mechanical properties were examined by using a hardness test, a tensile test, a Charpy impact test and a drop weight tear test (DWTT), respectively. The results show that the base metal (BM) of the pipe has a low yield ratio of 0.83 and an excellent elongation of more than 45%. The DWTT shear area of the steel plate reaches 87%, showing excellent low-temperature toughness. The Charpy impact energy increases when the distance from the fusion line increases, and it reaches a maximum at the BM near the heat-affected zone (HAZ) due to the small martensite-austenite (MA) constituents and fine grains. The concentrated distribution of blocky/slender MA constituents along the prior austenite grain boundaries of the intercritically reheated coarse-grained HAZ and the large MA constituents are the main reasons for the deteriorating impact toughness. Delamination cracks in the DWTT fracture surface only occurred in the midthickness of a sample with a small opening width that spread about 2.1 mm perpendicular to the DWTT fracture surface and were finally arrested at the acicular ferrite clusters containing a high density of high-angle boundaries.
About Me
Doctor of Zhengzhou University, mainly engaged in metal materials research.
Doctor of Zhengzhou University, mainly engaged in metal materials research.