This study investigated the thermomechanical behavior of 4D-printed polylactic acid (PLA), focusing on its response to varying temperatures and strain rates in a wide range below the glass transition temperature (Tg). The material was characterized using tension, compression, and dynamic mechanical thermal analysis (DMTA), confirming PLA’s strong dependency on strain rate and temperature. The glass transition temperature of 4D-printed PLA was determined to be 65 °C using a thermal analysis (DMTA). The elastic modulus changed from 1045.7 MPa in the glassy phase to 1.2 MPa in the rubber phase, showing the great shape memory potential of 4D-printed PLA. The filament tension tests revealed that the material’s yield stress strongly depended on the strain rate at room temperature, with values ranging from 56 MPa to 43 MPA as the strain rate decreased. Using a commercial FDM Ultimaker printer, cylindrical compression samples were 3D-printed and then characterized under thermo-mechanical conditions. Thermo-mechanical compression tests were conducted at strain rates ranging from 0.0001 s−1 to 0.1 s−1 and at temperatures below the glass transition temperature (Tg) at 25, 37, and 50 °C. The conducted experimental tests showed that the material had distinct yield stress, strain softening, and strain hardening at very large deformations. Clear strain rate dependence was observed, particularly at quasi-static rates, with the temperature and strain rate significantly influencing PLA’s mechanical properties, including yield stress. Yield stress values varied from 110 MPa at room temperature with a strain rate of 0.1 s−1 to 42 MPa at 50 °C with a strain rate of 0.0001 s−1. This study also included thermo-mechanical adiabatic tests, which revealed that higher strain rates of 0.01 s−1 and 0.1 s−1 led to self-heating due to non-dissipated generated heat. This internal heating caused additional softening at higher strain rates and lower stress values. Thermal imaging revealed temperature increases of 15 °C and 18 °C for strain rates of 0.01 s−1 and 0.1 s−1, respectively.
This paper deals with the selection of the optimal material for railway wagons, from among three different steel and three aluminium based materials, by using four different Multicriteria Decision Making Methods (MCDM) and comparing their ranking of the materials. We analysed: Dual-Phase 600 steel, Transformation-Induced Plasticity (TRIP) 700 steel, Twinning-Induced Plasticity (TWIP) steel, Aluminium (Al) alloys, Al 6005-T6, and Al 6082-T6, and porous Al structure with closed cells. Four different MCDM methods were used: VIKOR, TOPSIS, PROMETTHEE and the Weighted aggregated sum product assessment method (WASPAS). Key material properties that were used in the MCDM analysis were: density, yield strength (Y.S.), tensile strength (T.S.), Y.S./T.S. ratio, Youngs modulus (Y.M.), cost and corrosion resistance (C.R.). Research results indicate that aluminium and its alloys prove to be the most suitable material, based on setup criteria. Advanced steels also achieved good ranking, making them a valid option, immediately behind lightweight aluminium alloys. Porous aluminium did not perform well, according to the used MDCM methods, mainly due to the significantly lower strength exhibited by the porous structures in general.
We have studied an application of the Voronoi tessellation method in the modeling of open-cell aluminium foam under uniaxial compressive loading. The Voronoi code was merged with computer-aided design (CAD) for converting the polyhedral model into an irregular open-cell cellular structure to create porous samples for compression testing simulations. Numerical simulations of the uniaxial compression uniformly over the upper surface of the sample in the z-axis direction at a constant 20 N load was realised. Samples with three different porosities (30%, 60% and 80%) were studied. A nonlinear elasto-plastic material model with perfect plasticity, without hardening, based on the von Mises yield criterion was applied below 10% strain. Corresponding stress–strain curves were observed and the influence of porosity on deformation mechanism was discussed. Samples with higher porosity exhibited significantly higher normal stress under the same load, and increased stress plateaus. An increase of porosity produced an increase of both compressive and tensile stresses and struts exhibited complex stress fields. Voronoi-based modeling was in accordance with experimental results in the literature in the case of the quasi-static condition and linear elastic region (below 1% strain). Further study is necessary to enable the simulation of real dynamic behaviour under all deformation regimes by using the Voronoi tessellation method.
Flexoelectricity arises in materials under strain gradients, which can be particularly significant for situations in which the existence of other electromechanical properties is absent or generating large flexoelectric properties is achievable. This effect has also been observed in some biological materials, whose understanding can hugely help to further enhance our understanding of vital biological processes like mechanotransduction, as well as the development of applications in regenerative medicine and drug delivery. While the field of flexoelectricity as a relevant topic in biological materials is relatively new and still developing, the current study aims to review available results on flexoelectric effects in biological materials such as cells and cell membranes, hearing mechanisms, and bone, and their potential applications in biomedical research. Therefore, we first provide a brief background on two main electromechanical couplings (piezoelectricity and flexoelectricity) and further, how flexoelectricity has been experimentally and theoretically identified. We then review flexoelectricity in different biological materials as the main aim of the current study. Within that, we provide additional emphasis on the influence of this effect on bone and bone remodeling. In particular, the study outlines current limitations and provides potential directions for future work, emphasizing the crucial role in the development of next-generation electromechanical devices and optimizing their function in the area of biomedical research.
This study was conducted on different models of biodegradable SMP (shape-memory polymer) scaffolds. A comparison was conducted utilizing a basic FDM (fused deposition modeling)/MEX (material extrusion) printer with a standard printing technique and a novel, modified, four-axis printing method with a PLA (poly lactic acid) polymer as the printing material. This way of making the 4D-printed BVS (biodegradable vascular stent) made it possible to achieve high-quality surfaces due to the difference in printing directions and improved mechanical properties—tensile testing showed a doubling in the elongation at break when using the four-axis-printed specimen compared to the regular printing, of 8.15 mm and 3.92 mm, respectfully. Furthermore, the supports created using this method exhibited a significant level of shape recovery following thermomechanical programming. In order to test the shape-memory effect, after the thermomechanical programming, two approaches were applied: one approach was to heat up the specimen after unloading it inside temperature chamber, and the other was to heat it in a warm bath. Both approaches led to an average recovery of the original height of 99.7%, while the in-chamber recovery time was longer (120 s) than the warm-bath recovery (~3 s) due to the more direct specimen heating in the latter case. This shows that 4D printing using the newly proposed four-axis printing is an effective, promising technique that can be used in the future to make biodegradable structures from SMP.
This paper presents short review of the OCT technology concepts, including the recently emerging low-cost OCT devices. Technology concept of Fourier-domain OCT, based on spectral interferometry, is presented: spectral-domain OCT (SD-OCT) and swept-source OCT (SS-OCT). Technical properties of the recently developed low-cost OCT solutions are reviewed. Advanced OCT measurements in clinical ophthalmology are discussed, with relevant case studies. Further research directions that consider AI-based methods in OCT imaging is briefly presented.