In this study, basalt fiber-reinforced polymer (BFRP) composites with epoxy matrix, 20 layers, and volume fraction of fibers Vf = 53.66%, were prepared by a hand lay-up compression molding combined method. The fabric of the basalt fibers is in twill 2/2 weave. Through dynamic mechanical analysis (DMA), their viscoelastic behavior at elevated temperatures and in various frequencies was explored, whereas thermomechanical analysis (TMA) took part in terms of creep recovery and stress-relaxation tests. Moreover, the glass transition temperature (Tg) of the BFRP composites was determined through the peak of the tanδ curves while the decomposition of the BFRP composites and basalt fibers, in air or nitrogen atmosphere, was explored through thermogravimetric analysis (TGA). The mechanical behavior of the BFRP composites was investigated by tensile and three-point bending experiments. The results showed that as the frequency is raised, the BFRP composites can achieve slightly higher Tg while, under the same circumstances, the storage modulus curve obtains a less steep decrease in the middle transition region. Moreover, the hand lay-up compression molding hybrid technique can be characterized as efficient for the preparation of polymer matrix composites with a relatively high Vf of over 50%. Remarkably, through the TGA experiments, the excellent thermal resistance of the basalt fibers, in the temperature range 30–900 °C, was revealed.
22 May 2018 in IOP Conference Series: Materials Science and Engineering
In this study, aramid fiber-reinforced polymer (AFRP) composites were prepared and then postcured under specific heating/cooling rates. By dynamic mechanical analysis, the viscoelastic properties of the AFRP composites at elevated temperatures and under various frequencies were determined. Thermomechanical analysis (TMA), in the modes of creep-recovery and stress–relaxation tests, was also performed. Furthermore, differential scanning calorimetry was also used, and the decomposition of the AFRP composites, aramid fibers, and pure postcured epoxy, in two different atmospheres, namely, air atmosphere and nitrogen (N2) atmosphere, was explored by the thermogravimetric analysis (TGA). From this point of view, the aramid fibers showed remarkably thermal resistance, in N2 atmosphere, and the volume fraction of fibers (Φf) was calculated to be Φf = 51%. In the TGA experiments, the postcured AFRP composites showed very good thermal resistance, both in air and N2 atmosphere, and this characteristic in conjunction with their relatively high Tg, which is in the range of 85–95°C, depending on the frequency and the determination method, classifies these composites as potential materials in applications where the resistance in high temperatures is a required characteristic.
1 January 2020 in IOP Conference Series: Materials Science and Engineering
This article deals with the lifetime of laminated materials produced by different production technologies (hand lamination technology, vacuum bagging technology and prepreg technology with curing in the oven) during cyclic repeated bending stress. Like tested materials composite systems were chosen composite systems with epoxy matrix and carbon reinforcement (Kordcarbon CC200T, epoxy resin with trade name L285) and second composite epoxy system with glass reinforcement (Quadra-axial glass fabric, named Saertex Q-E-820, epoxy resin Biresin CR 82 and third prepreg systems (unidirectional prepreg, trade name Deltapreg VV430U-DT860W-39% and prepreg system with glass fabric VV320P_DT806R-37%). Fatigue tests were performed by cyclic bending loads during a three-point arrangement on a universal servo-hydraulic testing machine INSTRON 8871. Experimentally the number of cycles fracture of the material was determined at 90 % and 80 % of the maximum breaking load.