Gradient nanostructure (GNS) has drawn great attention, owing to the unique deformation and properties that are superior to nanostructure with uniform scale. GNS is commonly fabricated via surface plastic deformation with small tips (of balls or shots) so as to produce high deformation to refine the coarse grains, but unfortunately it suffers from the deterioration of surface quality which is hard to guarantee the reliable service. Although there are mirror-finishing techniques that can greatly enhance the surface quality, the induced slight deformation is commonly unable to produce GNS of reasonable thickness. Here, we propose a method to fabricate a GNS surface layer with a substantially enhanced surface quality via ultra-sonic rolling treatment (USRT), namely, surface rolling with a roller vibrated at a frequency of 20,000 Hz. It is found that 4-pass USRT is able to produce 20–30 µm thick GNS on AISI 304 stainless steel pipe inner surface, wherein the surface quality is enhanced by one order of magnitude from the starting Ra = 3.92 µm to 0.19 µm. Processing by a roller with a high-frequency vibration is necessary for both good surface quality and the effective accumulation of heavy deformation on the surface. The flattening mechanism as well as the microstructural evolution from millimeter- to nanometer-scale for AISI 304 stainless steel is discussed.

To solve the problem of poor weldability between TiAl-based and Ti₂AlNb-based alloys, spark plasma diffusion bonding was employed to join a TiAl alloy and a Ti₂AlNb alloy with a pure Ti foil as interlayer at 950 °C/10 KN/60 min. After welding, slow cooling was carried out at a rate of 5 °C/min, followed by homogenization at 800 °C for 24 h. The microstructural evolution and elemental migration of the joint were analyzed via a scanning electron microscope equipped with an energy dispersive spectrometer, while the mechanical properties of the joint were assessed via microhardness and tensile tests. The results show that the spark plasma diffusion bonding formed a joint of TiAl/Ti/Ti₂AlNb without microcracks or microvoids, while also effectively protecting the base metal. Before heat treatment, the maximum hardness value (401 HV) appeared at the Ti₂AlNb/Ti interface, while the minimum hardness value (281 HV) occurred in the TiAl base metal. The tensile strength of the heat-treated joint at room temperature was measured to be up to 454 MPa, with a brittle fracture occurring in the interlayer. The tensile strength of the joint at 650 °C was measured to be up to 538 MPa, with intergranular cracks occurring in the TiAl base metal.

This study investigated the use of oscillating laser welding with Cu, Mo, and Nb interlayers to mitigate the issue of brittle intermetallic compound (IMC) formation in titanium-steel dissimilar welding for TC4/304SS lap joints. This study systematically examined the influence of interlayer type on joining mechanisms, microstructure, and mechanical properties. Results indicated that direct welding produced Ti-Fe IMCs (TiFe phase) through fusion, resulting in a thick brittle layer. The Cu interlayer facilitated fusion welding while promoting the formation of TiFe₂ and TiCu₄ phases. Mo and Nb interlayers, through fusion-brazing and brazing mechanisms, respectively, inhibited Ti-Fe IMCs by generating Fe-Mo/Nb IMCs and (Ti, Mo/Nb) solid solutions. Mechanical testing indicated that Mo-interlayer joints exhibited the highest shear strength at 1129.53 N, representing a 31% increase relative to direct joining. This was followed by Nb at 1004.4 N, Cu at 871.6 N, and direct welding at 859.13 N. Fracture transitioned from brittle IMC layers in Cu and direct welding to interfaces between interlayers and TC4 in Mo and Nb systems. This study presents Mo/Nb interlayers as the most effective choice for high-strength Ti-steel joints, providing insights for the selection of interlayers in engineering applications.