Alloyed Ductile iron, austenitized at 840 °C for 30 min in a special sealed austempering furnace, was austempered for 30 min in molten salt mixture at 4 trial temperatures of 300 °C, 320 °C, 340 °C and 360 °C. Tensile strength, yield strength, percentage elongation and impact energy were evaluated for the as-cast and austempered samples. Microstructures were investigated using microscopy, coupled with analyzing software and a scanning electron microscopy. The specific wear of samples was tested using pin-on-disc wear testing machine. X-ray diffraction was performed to calculate the amount of retained austenite present in the ausferrite matrix. As-cast microstructure consists of ferrite and pearlite, whereas austempered ductile iron (ADI) contains a mixture of acicular ferrite and carbon enriched austenite, called “ausferrite”. Hardness and strength decreased, whereas ductility and impact strength improved with an increase in the austempering temperature. XRD analysis revealed that the increase in austempering temperature increased the retained austenite content. A decrease in wear resistance with austempering temperature was observed. Modified Quality Index (MQI) values were envisaged, incorporating tensile strength, elongation and wear resistance. MQI for samples austempered at 340 °C and 360 °C showed a better combination of properties. About an 8% reduction in energy consumption was gained when the heat treatment parameters were optimized.
Hybrid laminates made using natural fibers have been finding applications in diverse fields such as automotive parts, building structures and sports goods. These laminates incorporate the benefits of the reinforcements used in constructions. The present work deals with the fabrication of hybrid laminate comprising of the natural fibers areca and kenaf in varying stacking sequences through the hand layup method. Epoxy resin (LY556) and hardener (HY951) are mixed in the ratio of 10:1 to prepare the matrix material. Six different hybrid laminates having five layers of areca and kenaf in different stacking sequences are produced. Two more laminates having either kenaf or areca in all the five layers and are produced to act as reference laminate. The prepared laminates are cut as per ASTM standards and subjected to tensile, compressive, flexural, impact and hardness tests in order to identify the properties of the fabricated laminates. The result shows that composite made with kenaf fiber as skin material and areca as core materials exhibit better tensile, flexural and hardness properties. Likewise, composites with outer layers of areca and core layers of kenaf fibers have high compressive and impact strength. The fractured surfaces after the mechanical tests are investigated through the Scanning Electron Microscope (SEM).
Strip cast samples with different copper content have been developed by simulated direct strip casting. The as-cast microstructures were characterized by optical microscopy and electron microscopy. The microstructures mainly consisted of polygonal ferrite and Widmanstatten ferrite in as cast condition. X-ray diffraction showed that the copper was in solid solution in the as-cast condition. It was found that the equivalent tensile yield and maximum strengths, both increased with an increase in copper content. The strip cast samples were cold rolled to 70% reduction and then annealed isothermally at 600, 650 and 700 °C for various times to study the recrystallization and precipitation kinetics. After annealing, the hardness and strength were found to be decreased due to recovery and recrystallization. It was found that an increase in copper content retarded the recrystallization kinetics. During annealing, precipitation of copper was observed. The copper precipitates were bimodal with respect to particle size and distribution. The size and spacing of the particles were measured and the Zener pinning effect of the particles was calculated. High pinning forces of more than 2 MPa were predicted, and this correlated well with the observed decrease in recrystallization kinetics.