Ceramics have excellent properties such as hardness and thermal and chemical stability. Therefore, researchers have studied the use of 3D printing to produce complex shapes in tools and structural applications. The debinding and sintering processes for ceramic composite materials manufactured using digital light processing (DLP) 3D printing technology were studied. The slurry used for DLP 3D printing requires debinding and sintering, as it contains ceramics and binders. Therefore, the debinding and sintering processes were measured by TG-DSC curves, and the changes in material characteristics were evaluated by setting the debinding holding time (4, 5, and 6 h) and sintering temperature (1100, 1200, and 1300 °C) as parameters. After debinding for 6 h, the density of the ceramic sintered at 1300 °C was 1.36 g/cm²; the linear shrinkage was 22.1%/21.6%/28.5% along the x, y, and z axes, respectively; and the bending strength was 8.58 MPa. As a result of this study, we developed an optimized process for the debinding and sintering of ceramics manufactured through the DLP 3D printing process.

In this study, a room-temperature ammonia gas sensor using a ZnO and reduced graphene oxide (rGO) composite is developed. The sensor fabrication involved the innovative application of reverse offset and electrostatic spray deposition (ESD) techniques to create a ZnO/rGO sensing platform. The structural and chemical characteristics of the resulting material were comprehensively analyzed using XRD, FT-IR, FESEM, EDS, and XPS, and rGO reduction was achieved via UV–ozone treatment. Electrical properties were assessed through I–V curves, demonstrating enhanced conductivity due to UV–ozone treatment and improved charge mobility from the formation of a ZnO–rGO heterojunction. Exposure to ammonia gas resulted in increased sensor responsiveness, with longer UV–ozone treatment durations yielding superior sensitivity. Furthermore, response and recovery times were measured, with the 10 min UV–ozone-treated sensor displaying optimal responsiveness. Performance evaluation revealed linear responsiveness to ammonia concentration with a high R² value. The sensor also exhibited exceptional selectivity for ammonia compared to acetone and CO gases, making it a promising candidate for ammonia gas detection. This study shows the outstanding performance and potential applications of the ZnO/rGO-based ammonia gas sensor, promising significant contributions to the field of gas detection.

This paper reports a high-performance humidity sensor made using a novel cellulose nanofiber (CNF)–silver nanoparticle (AgNP) sensing material. The interdigital electrode pattern was printed via reverse-offset printing using Ag nano-ink, and the sensing layer on the printed interdigitated electrode (IDE) was formed by depositing the CNF-AgNP composite via inkjet printing. The structure and morphology of the CNF-AgNP layer are characterized using ultraviolet–visible spectroscopy, an X-ray diffractometer, field emission scanning electron microscopy, energy-dispersive X-ray analysis, and transmission electron microscopy. The humidity-sensing performance of the prepared sensors is evaluated by measuring the impedance changes under the relative humidity variation between 10 and 90% relative humidity. The CNF-AgNP sensor exhibited very sensitive and fast humidity-sensing responses compared to the CNF sensor. The electrode distance effect and the response and recovery times are investigated. The enhanced humidity-sensing performance is reflected in the increased conductivity of the Ag nanoparticles and the adsorption of free water molecules associated with the porous characteristics of the CNF layer. The CNF-AgNP composite enables the development of highly sensitive, fast-responding, reproducible, flexible, and inexpensive humidity sensors.

The performance, stability, and lifespan of lithium-ion batteries are influenced by variations in the flow of lithium ions with temperature. In electric vehicles, coolants are generally used to maintain the optimal temperature of the battery, leading to an increasing demand for temperature and humidity sensors that can prevent leakage and short circuits. In this study, humidity and temperature sensors were fabricated on a pouch film of a pouch-type battery. IDE electrodes were screen-printed on the pouch film and humidity- and temperature-sensing materials were printed using a dispenser process. Changes in the capacitance of the printed Ag-CNF film were used for humidity sensing, while changes in the resistance of the printed PEDOT:PSS film were used for temperature sensing. The two sensors were integrated into a single electrode for performance evaluation. The integrated sensor exhibited a response of ΔR ≈ 0.14 to temperature variations from 20 °C to 100 °C with 20% RH humidity as a reference, and a response of ΔC ≈ 2.8 to relative humidity changes from 20% RH to 80% RH at 20 °C. The fabricated integrated sensor is expected to contribute to efficient temperature and humidity monitoring applications in various pouch-type lithium-ion batteries.