In response to the growing demand for high-sensitivity accelerometers in vector hydrophones, a piezoelectric MEMS accelerometer (PMA) was proposed, which has a four-cantilever beam integrated inertial mass unit structure, with the advantages of being lightweight and highly sensitive. A theoretical energy harvesting model was established for the piezoelectric cantilever beam, and the geometric dimensions and structure of the microdevice were optimized to meet the vibration pickup conditions. The sol-gel and annealing technology was employed to prepare high-quality PZT thin films on silicon substrate, and accelerometer microdevices were manufactured by using MEMS technology. Furthermore, the MEMS accelerometer was packaged for testing on a vibration measuring platform. Test results show that the PMA has a resonant frequency of 2300 Hz. In addition, there is a good linear relationship between the input acceleration and the output voltage, with V = 8.412a − 0.212. The PMA not only has high sensitivity, but also has outstanding anti-interference ability. The accelerometer structure was integrated into a vector hydrophone for testing in a calibration system. The results show that the piezoelectric vector hydrophone (PVH) has a sensitivity of –178.99 dB@1000 Hz (0 dB = 1 V/μPa) and a bandwidth of 20~1100 Hz. Meanwhile, it exhibits a good “8” shape directivity and consistency of each channel. These results demonstrate that the piezoelectric MEMS accelerometer has excellent capabilities suitable for use in vector hydrophones.

High-performance vector hydrophone that can acquire underwater acoustic vector information is crucial to the effectiveness of underwater target monitoring. In this paper, a novel piezoelectric MEMS vector hydrophone (PMVH) is proposed with d₃₁ working mode, which has a cross-beam integrated microsphere structure. The passive acoustic receiving unit has been integrated for a low-density microsphere instead of the ordinary cilium by increasing the sensing area of the receiving unit. Heterogeneous integrated preparation of high quality PbZr _0.52 Ti _0.48 O ₃ (PZT) thin film was realized on the cross-beam by sol-gel technology. The optimized geometric size of the sensitive structure was determined by simulation analysis. Based on the optimized parameters, the MEMS technology was employed to fabricate the hydrophone microdevices, and a prototype of the PMVH has been assembled. The PMVH is verified experimentally in a standing bucket wave calibration system. The experimental results show that compared to the bionic cilia MEMS vector hydrophone (CVH) the receiving sensitivity reaches up to -177.71 dB (re 1V/μPa) at 1000 Hz, which is higher than 19.3 dB,. Moreover, the bandwidth of the PMVH reaches 20Hz~1150Hz, which exhibits a satisfactory 8-shaped directivity. The results of this work pave a new way to development of piezoelectric hydrophone for underwater communications and acoustic monitoring.

Expandable graphite (EG) was modified with a charring agent and organic–inorganic hybridized intumescent flame retardants (MEG) were synthesized. This study uses a cone calorimeter (CCT) and a DaqPRO 5300 radiation heat flow meter (Fourtec, Tel Aviv, Israel) to evaluate the fire-resistant properties influenced by MEG on intumescent fire-retardant coatings. The impact of MEG on the thermal degradation of these coatings was investigated through the use of thermogravimetric analysis (TGA). The results obtained by CCT demonstrated that the incorporation of MEG markedly diminished the heat release rate and total heat release rate of the coating, in addition to enhancing the char residue compared to coatings with only expandable graphite (EG). Furthermore, TGA results demonstrate that adding MEG increases the weight of the char residue at elevated temperatures, suggesting improved thermal stability. Based on these findings, MEG exhibits a synergistic flame-retardant effect when combined with intumescent fire-retardant (IFR) systems. This synergy not only improves the flame-retardant properties of the coatings but also enhances their overall thermal stability, making MEG a promising additive for developing more efficient fire-retardant materials. Thus, MEG-modified coatings offer superior protection against fire hazards, highlighting their potential for practical applications in fire safety.

The 2524-T3 aluminum alloy was subjected to fatigue tests under the conditions of R = 0, 3.5% NaCl corrosion solution, and the loading cycles of 10⁶, and the S-N curve was obtained. The horizontal fatigue limit was 169 MPa, which is slightly higher than the longitudinal fatigue limit of 163 MPa. In addition, detailed microstructural analysis of the micro-morphological fatigue failure features was carried out. The influence mechanism of corrosion on the fatigue crack propagation of 2524-T3 aluminum alloy was discussed. The fatigue source characterized by cleavage and fracture mainly comes from corrosion pits, whose expansion direction is perpendicular to the principal stress direction. The stable propagation zone is characterized by strip fractures. The main feature of the fracture in the fracture zone is equiaxed dimples. The larger dimples are mixed with second-phase particles ranging in size from 1 to 5 μm. There is almost a one-to-one correspondence between the dimples and the second-phase particles. The fracture mechanism of 2524 alloy at this stage is transformed into a micro-holes connection mechanism, and the nucleation of micropores is mainly derived from the second-phase particles.

Electric field-assisted sintering has ubiquitous merits over conventional sintering technology for the fabrication of difficult-to-deform materials. To investigate the effect of sintering pressure and temperature on the densification of Inconel 718 superalloy, a numerical simulation model was established based on the Fleck-Kuhn-McMeeking (FKM) and Gurson-Tvergaard-Needleman (GTN) models, which covers a wide range of porosity. At a sintering pressure below 50 MPa or a sintering temperature below 950 °C, the average porosity of the sintered superalloy is over 0.17 with low densification. Under a pressure above 110 MPa and a temperature above 1250 °C, the sintered superalloy quickly completes densification and enters the plastic yield stage, making it difficult to control the sintering process. When the pressure is above 70 MPa while the temperature exceeds 1150 °C, the average porosity is 0.11, with little fall when the pressure or temperature rises. The experimental results indicated that the relative density of the sintered superalloy under 70 MPa and 1150 °C is 94.46%, and the proportion of the grain size below 10 μm is 73%. In addition, the yield strength of the sintered sample is 512 MPa, the compressive strength comes to 1260 MPa when the strain is over 0.8, and the microhardness is 395 Hv, demonstrating a better mechanical property than the conventional superalloy.

Metal oxide semiconductors (MOSs) hold great promise for electronic devices such as gas sensors. The utilization of ZnO as a conductometric gas sensor material can be traced back to its early stages; however, its application has primarily been limited to high-temperature environments. A gas sensor based on highly porous and interconnected 3D networks of ZnO tetrapod (ZnO-T) micro-nano structures was fabricated via an easy chemical vapor deposition (CVD) method. Homemade instruments were utilized to evaluate the gas-sensing of the sample at room temperature. It exhibited good gas-sensing at room temperature, particularly with a response of up to 338.80% toward 1600 ppm ethanol, while also demonstrating remarkable repeatability, stability, and selectivity. Moreover, the unique gas-sensing properties of ZnO-T at room temperature can be reasonably explained by considering the effect of van der Waals forces in physical adsorption and the synergistic effect of carrier concentration and mobility. The aforementioned statement presents an opportunity for the advancement of gas sensors utilizing ZnO at room temperature.