The recovery behavior and selected mechanical properties were studied for Populus tomentosa wood subjected to surface compression followed by heat treatment. The surface compression of wood was carried out in an open hot-pressing system at 180 °C with compressed thickness of 2 to 18 mm. The surface-compressed wood was treated by atmospheric heat treatment or 0.30 MPa pressurized superheated-steam heat treatment at 180 °C for 2 h. The results showed that the set recovery of compressed wood decreased with increasing compressed thickness before post-treatment. Atmospheric and pressurized heat treatment reduced the average set recovery of compressed wood significantly from 12.9% to 4.1% and 1.5% respectively, after conditioning at 40 °C and 90% relative humidity. Moreover, mechanical properties including the modulus of elasticity (MOE), modulus of rupture (MOR), hardness, and surface hardness increased with elevating compressed thickness. Both atmospheric and pressurized heat treatment reduced the MOR, hardness, and surface hardness of compressed wood. Analysis of variance showed that the effects of heat treatment on mechanical properties was not significant, except pressurized heat treatment decreased hardness significantly. With a compressed thickness of 10 mm, MOE, MOR, hardness and surface hardness were increased by 52.6%, 36.4%, 122.0% and 129.6%, respectively, compared with untreated wood.

The combination of surface densification and superheated steam treatment is an effective method to improve the mechanical properties and dimensional stability of low-density wood. The objective of the current work is to evaluate the effects of superheated steam treatment on the micromechanical behavior of surface densified wood. The microstructure, chemical composition, cellulose crystalline structure, and micromechanical behavior of surface densified wood under different superheated steam pressures were investigated. Results indicated that both 0.1 MPa and 0.3 MPa superheated steam treatments increased the elastic modulus and hardness of fiber cell walls in surface densified wood. However, the average creep ratio and maximum creep compliance J(50) of surface densified wood under 0.3 MPa decreased by 41.59% and 6.76%, respectively, compared with untreated wood. The improvement of elastic modulus, hardness and creep resistance of surface densified wood treated with superheated steam was associated with the increase of relative crystallinity (CrI) and crystalline size. In addition, 0.3 MPa superheated steam treatment displayed a better effect on the enhancement of the elastic modulus, hardness, and creep resistance of the fiber cell wall than 0.1 MPa superheated steam treatment.

In this study, twenty-five heat treatments were conducted at the various treating conditions of five temperatures and five durations. At each treatment, 15 poplar specimens were used. Twelve variables that represented wood color, physical and mechanical properties and durability were measured for both treated and untreated specimens. To evaluate the effect of heat treatment on the wood performance, a comprehensive cluster analysis was applied to the measured variables of treated and untreated specimens. Cluster analysis showed that treating and control specimens can be distinctly classified into 2, 3 or 4 clusters according to the intended purposes. Two clusters can represent the control group and twenty-five testing groups. Four clusters represented the control group and three groups of testing specimens having mild, moderate and severe treating conditions, respectively. At the mild treatment, modulus of rupture (MOR) was reduced <11 %. Wood durability increased to moderate resistant. At the moderate treatment, EMC decreased by 28 %, and MOR was decreased by more than 12 %. In the severe treatment, wood durability increased to resistant or highly resistant; however, its MOR was reduced half.