In this study, we describe a sedimentary deposit situated above Ascunsă Cave (SW Romania) that should be in depositional connection with coeval stalagmites from the cave. We excavated a 2.5 m deep soil profile and took contiguous bulk samples every 5 cm. Soil samples were analyzed for clay mineralogy, grain size, chemical composition, magnetic susceptibility, and stable carbon isotopes. Radiocarbon dating revealed that the soil is of Holocene age, and presents a depositional hiatus between 5.4 and 2.3 thousand years before the present. Due to the open system behavior of soils and mobility of organic matter, a few hundred years of uncertainty should be considered for the duration of this hiatus. The fine fraction is dominated by silt, while the clay mineralogical association is made of illite, chlorite, kaolinite, vermiculite, and illite–vermiculite and illite–chlorite mixed layered minerals. The sediment source of this soil is represented by a nearby mélange complex, as well as by an underlying terra rossa-type soil. As this latter type of soil is widespread in our study area, we performed luminescence dating on two samples from a representative location close to our site and it appears that this type of Mediterranean soil was formed during the Last Interglacial period. δ¹³C variability in soil organic matter and a stalagmite from the cave are comparing well, and could help future studies identify modifications in isotopic fractionation processes within the cave.

The stone Ensemble from Corbii de Piatrǎ Romania arouses a continuous scientific interest, with the final goal being to obtain an exhaustive and multidisciplinary package of results that will become the support of an extensive restoration project. The cave painting stands out as the most important and most affected by the advanced degradation among the historical monuments in Romania. This article provides for the first time a radiocarbon dating of the first forms of painting by establishing the age of the mortar/plaster used as a pictorial support. Being a very complex context from the point of view of the type of datable material and the disappearance over time through degradation of other elements that would ensure a simpler and more reliable radiocarbon dating (such as the straws used to form the material), it was necessary to use a multidisciplinary approach for the selection of samples and for supporting the radiocarbon results. The set of analyses consisted of visualization techniques through microscopy and compositional analysis, providing information on the similarities/differences between the samples, the degradation mechanisms/impurities and the quality of the calcium carbonate dated by the Accelerator Mass Spectrometry (AMS) technique. The results supported each other, ensured the selection of reliable radiocarbon data and established the most probable moment of the early interventions, namely the two phases corresponding to the 14th century.