The Fatimid state was established in Egypt in 969 and lasted until the end of the dynasty in 1171. During the Fatimid rule in Egypt, a large set of monuments were erected. A significant portion of these monuments were shrines dedicated to the descendants of the Prophet Muhammed, especially in Aswan. Groundwater rising, at present, has introduced severe deterioration to the ancient earthen mud-brick architecture of the Fatimid tombs in Aswan city (Egypt). However, monitoring the influence of anthropogenic and environmental aspects on the deterioration issues in Fatimid tombs has not yet been considered. To this end, the scope of this pilot study is to investigate the structural stability and weathering vulnerability of the building materials of mud-brick structures in the Fatimid Cemetery before restoration labor. This was achieved using an integration of remote sensing (Landsat 8 and SRTM-DEM) and hydrogeological datasets in the Geographic Information System (GIS), along with a physicochemical and mineralogical analysis of various materials (the bearing soil, wall plasters, and Muqarnas) from the affected cemeteries. The morphological and mineralogical compositions of the collected samples were analytically examined by using X-ray diffraction (XRD) and scanning electron microscopy with energy dispersive X-ray spectroscopy (SEM/EDX) and CT scan. Moreover, geotechnical studies were conducted for the perched soil water and subsoil, including the analysis of the physiochemical composition and heavy metals using Inductively Coupled Plasma Mass Spectrometry (ICP-MS). The results of multitemporal analysis of land use/land cover (LULC) changes displayed the growth and appearance of wetlands near the Fatimid tombs area over the last decades, boosting the geo-environmental risks from soil water rising. Furthermore, the detailed analytical investigations of building materials and soil foundations showed that this unique and substantial ancient Islamic archaeological site of Egypt shows weak geotechnical properties, and it is highly sensitive to natural and anthropogenic stressors. This innovative methodology can produce novel recommendations and results to the Ministry of Antiquities in Egypt and the Heritage Commission in Saudi Arabia for the adequate restoration of monuments.

This paper presents a novel concept for significantly enhancing the strength and durability of ancient closed-box tombs. These tombs hold significant philosophical values, and their architecture serves as a valuable data source, providing insights into the cultural stage of the society in which it was constructed. Throughout medieval and modern times, clay bricks remained a prevalent material for tomb construction due to their affordability and design flexibility. However, these structures currently face neglect and weakening, requiring imperative intervention of protection to prevent them from potential deterioration or extinction. The key objective of this research is to explore the potential use of graphene oxide (GO), a novel nanomaterial, as a treatment method to enhance the durability of mud brick tombs in Aswan, Egypt. Samples of mud bricks were examined and characterized using various techniques, including SEM-EDX, TEM, PLM, XRF, XRD, and mechanical properties analysis. The results indicated that GO nanomaterials significantly improve the mechanical properties of mud brick tombs, allowing them to resist more compressive loading and ultimately resulting in more durable and long-lasting structures. By using these innovative materials, effective restoration and preservation of these ancient structures for future generations could be viable. This research has the potential to revolutionize the preservation of closed-box tombs, ensuring these historical landmarks stand longer the test of time.

This study evaluates a SiO₂ nanoparticle (SiO₂NPs)/Paraloid B-72 nanocomposite as a restorative and antifungal treatment for deteriorated sandstone at the Ptolemaic Temple of Isis, located within a densely populated residential area. The temple stones exhibit structural damage, soiling, and severe microbiological deterioration. Fungal isolates from the sandstone were cultured on PDA medium and identified by ITS region DNA sequencing as Alternaria alternata, Penicillium chrysogenum, and Aspergillus niger. The SiO₂NPs and their Paraloid B-72 nanocomposites were synthesized and characterized using transmission electron microscopy (TEM) and X-ray diffraction (XRD). Stone samples, examined before and after treatment via SEM-EDX, TEM, and XRD, were used to assess both conservation performance and compatibility. Laboratory antifungal tests showed that SiO₂NPs at 300 ppm exhibited the greatest inhibition of mycelial growth, reaching 91.59% for P. chrysogenum, 90.77% for A. niger, and 85.2% for A. alternata. Mechanical testing demonstrated that treatment with the SiO₂NPs/Paraloid B-72 nanocomposite enhanced stone strength, increasing compressive strength from 26.5 MPa to 27.4 MPa. SEM images confirmed excellent, homogeneous dispersion of the nanocomposite on stone grains, forming a coherent coating without pore occlusion. Overall, the SiO₂NPs/Paraloid B-72 formulation improved sandstone surface properties while substantially improving short-term mechanical performance and antifungal efficacy, indicating promise for enhancing restoration procedures when combined with established conservation protocols for sandstone architectural heritage.