By applying 2205 duplex stainless steel powders to repair and improve carbon steel, multi-pass laser-cladding tests were conducted on Q235 carbon steel surfaces with different laser powers in the range of 1.9~2.5 kW in order to evaluate the performance of the laser-cladding layers. The phase composition, macro- and microstructure, electrochemical corrosion resistance, friction, and wear resistance of the laser-cladding layers were investigated. Macroscopic observation identified no obvious cracks. The phases that made up the multi-pass laser-cladding layers were γ-Fe and α-Fe. Owing to the optimal laser power at 2.3 kW, a large number of equiaxed crystals and a small number of cellular crystals made up the microstructure of the prepared laser-cladding layer, which contributed to its good corrosion resistance. The wear resistance of the multi-pass laser-cladding layer and the carbon steel was also studied. A combined action of adhesive wear and abrasive wear, accompanied by oxidative wear, was determined through observation of pits and furrows on the friction surface of the multi-pass laser-cladding layer, while a typical mechanism of abrasive wear was confirmed by checking the friction surface of the carbon steel.
IrOx electrodes were fabricated by cyclic thermal heating and water quenching (CHQ) process and high temperature carbonate oxidation (HCO), respectively. By examining the E-pH relationship, response rate, potential drift behavior of the fabricated electrodes, the electrodes prepared by CHQ process seemed to show better comprehensive performance. Characterization tests such as scanning electron microscopy (SEM), X-ray photoelectron spectroscopy (XPS), Raman spectroscopy, and electrochemical impedance spectroscopy (EIS) were used to characterize the fabricated IrOx electrodes and find out the reason for the better performance of the electrodes prepared by CHQ process. Morphology tests indicate that the CHQ electrode shows a multi-layer structure with more ion channels, which could provide larger surface area for the H+ response process. Furthermore, combining the XPS, Raman and EIS tests etc., more effective response composition, better crystal quality, and smaller response reaction resistance of surface IrOx film could account for the better performance of the CHQ-fabricated IrOx electrode. The film formation process, H+ response mechanism, as well as the response behavior difference between the two kinds of the electrodes are further elaborated.