This study analyzes the behavior under the static delamination and mode-I fracture stress of adhesive joints made on the same composite material with an epoxy matrix and unidirectional carbon fiber reinforcement and two types of adhesives, one epoxy and the other acrylic. Standard DCB tests (for mode-I fracture) were used to quantify the influence on the interlaminar fracture toughness of the type of adhesive used. Both materials were subjected to two different degradation processes, one hygrothermal and the other in a salt-fog chamber. After aging, the mode-I fracture has been evaluated for both materials. From the experimental results obtained, it can be deduced for the epoxy adhesive that exposure to the hygrothermal environment used moderately modifies its behavior against delamination, while its exposure to the saline environment produces a significant loss of its resistance to delamination. For the acrylic adhesive, the hygrothermal exposure causes an improvement in its delamination behavior for all the exposure periods considered, while the saline environment slightly modifies its behavior. There is, therefore, a clear influence of the type of aging on the fracture behavior of both adhesives.

The present paper studies the fatigue delamination behaviour of an epoxy/carbon composite material under mode III loading using a longitudinal half fixed beam (LHFB) device initially designed for mode III static tests of composite materials formed by the stacking of plies. For this purpose, a series of tests was carried out at different levels of loading representative of the fatigue behaviour of the material, from the crack onset phase through the delamination phase to final fracture. The experimental results were treated statistically, obtaining the values of the fatigue limit for probabilities of fracture of 5% and 50%. Finally, a fractographic analysis of the fracture surfaces was performed which allowed us to identify the same characteristic patterns of static mode III fracture, namely broken fibres, cusps and saw-teeth, in addition to a new morphology consisting of the formation of agglomerations of resin produced by the friction between the lips of the specimen in the fracture zone that point to dynamic mode III fracture. These agglomerations eventually crack and become detached from the fibres, leaving these free of resin.

The Asymmetric Double Cantilever Beam (ADCB) is a common test configuration used to produce mixed mode I/II in composite materials. It consists of two sublaminates with different thicknesses or elastic properties, a situation that usually occurs in bimaterial adhesive joints. During this test, the sample undergoes rotation. In this work, the influence of this rotation on the calculation of the energy release rate (ERR) in modes I and II was studied using the Finite Element Method (FEM). Several models with different degrees of asymmetry (different thickness ratio and/or elastic modulus ratio) and different applied displacements were prepared to obtain different levels of rotation during the test. As is known, the concept of modes I and II refers to the components of the energy release rate calculated in the direction perpendicular and tangential to the delamination plane, respectively. If the model experiences significant rotation during the application of the load, this non-linearity must be considered in the calculation of the mode partition I/II. In this work, appreciable differences were observed in the values of modes I and II, depending on their calculation in a global system or a local system that rotates with the sample. When performing crack growth calculations, the difference between critical loads can be in the order of 4%, while the difference between mode I and mode II results can reach 4% and 14%, respectively, for an applied displacement of only 5 mm. Currently, this correction is not usually implemented in Finite Element calculation codes or in analytical developments. The purpose of this article is to draw attention to this aspect when the rotation of the specimen is not negligible.