The aim of the present study was to extract starch from acorn (Quercus suber L.) fruits using water and alkaline methods. Structural and functional properties of extracted starches were investigated and compared to those of corn and modified starches in order to determine their innovative potential application in food industry. The yield of extraction using the two methods was about 48.32% and 48.1%. The isolated starches showed low moisture, fat and protein contents, revealing high purity and quality. Additionally, the starch extracted using the alkaline method (AAS) showed higher lightness (60.41) when compared to starch isolated using hot water (WAS). However, the lightest white color was found for studied commercial starches. Moreover, AAS starch exhibited the highest swelling power, solubility and water absorption, followed by WAS and commercial starches. Results showed that extracted acorn starches were characterized by greater enthalpy and gelatinization temperatures. Similar observations were noted using FT-IR spectra analysis for all analyzed starches. In addition, granule starches observed using scanning electron microscopy were found to be spherical and ovoid. However, from the analysis by X-ray diffraction, a crystalline pattern of C-type was found for acorn starches, while commercial starches presented an A-type pattern. As an innovative food application, these underexploited acorn starches were valued and served to produce new custards with improved functional properties and better microstructure when compared to commercial custard.

In this study, a new starch has been isolated from acorn (Quercus ilex) fruits. The chemical composition of acorn flour showed its richness in carbohydrates (64.43%), proteins (8%), and fat (10%). The extraction yield of acorn starch was about 34.5%. Thus, the composition of extracted acorn starch and its physical and functional properties were studied. Acorn starch had high purity represented by low proportions of proteins (0.92%) and lipids (0.51%) with a pH of 5.3. The swelling power was 20.76 g/g, while the solubility was about 64.22% at 90°C which suggests that acorn starch has potential for use in food industries. The FT-IR spectra of isolated native starches have shown the main bands characterizing the starch. However, X-ray diffractograms exhibited an A- and B-type diffraction pattern. Furthermore, the effect of acorn starch incorporation at different levels (0.5%, 1%, 1.5%, and 2%) on the quality parameters of a fermented dairy product was investigated at the beginning of storage. The results demonstrated that the most suitable dose of acorn starch to be incorporated in the fermented dairy product was lower than 1%. This low concentration reduced syneresis, improved functional properties, and enhanced the viscosity of the fermented dairy product.

Gluten-free (GF) baked goods often lack nutritional balance due to the limited protein and fiber content of standard cereal flours like rice and maize. A mixture design methodology was used to evaluate the interaction effects between cereal and legume flours on the physical and textural properties of the biscuits, including hardness, water activity (aw), CIE color parameters (L*, a*, and b*), spread ratio, and baking loss. The results indicated that incorporating legume flour, particularly chickpea flour, significantly increased biscuit hardness (from 22.00 N to 34.66 N) and reduced water activity (from 0.23 to 0.17). All three legume flours reduced the spread ratio, with chickpea flour having the most pronounced effect (from 4.91 to 4.75). Nutritionally, the inclusion of legume flours improved the protein (from 6.46 g/100 g to 11.90 g/100 g), mineral (from 0.58 g/100 g to 1.25 g/100 g), fiber (from 15.73 g/100 g to 21.13 g/100 g), and polyphenol contents (0.34 mg GAE/g compared to 0.18 mg GAE/g for the control). Moreover, DPPH scavenging activity was significantly higher (72.72% vs. 31.49% for the control). Sensory evaluations indicated that the inclusion of legume flours positively affected the biscuits’ overall sensory attributes, especially appearance, but had a minor negative effect on texture. This study aimed at utilizing local legume flours: faba bean, chickpea, and lentil, besides the traditional standard flours: rice and maize, to develop nutritious and flavorful gluten-free biscuits. These results highlighted the use of combinations of local legume with cereal flours to produce GF biscuits with improved physical, sensory, and nutritional qualities.

The objective of this study was to determine the influence of two types of dryers (hot air oven and vacuum dryer) and the yellow berry percentage (1.75%, 36.25%, 43.25%) on the drying process and phytochemical content of bulgur. Results showed that the Midilli model successfully described the moisture diffusion during drying at 60 °C in all bulgur samples, where an increase in yellow berry percentage generated an increase in moisture content. Effective diffusion coefficient (D_eff) increased significantly (p ≤ 0.05) from 7.05 × 10⁻¹¹ to 7.82 × 10⁻¹¹ (m².s⁻¹) and from 7.73 × 10⁻¹¹ to 7.82 × 10⁻¹¹ (m².s⁻¹) for the hot air oven and vacuum dryer, respectively. However, it decreased significantly with a decrease of yellow berry percentage. It was concluded that the vacuum dryer provided faster and more effective drying than the hot air oven. Total polyphenol (TPC), total flavonoid (TFC), and yellow pigment contents (YPC) of bulgur were investigated. TPC ranged between 0.54 and 0.64 (mg GAE/g dm); TFC varied from 0.48 to 0.61 (mg QE/g dm). The YPC was found to be between 0.066 and 0.079 (mg ß-carotene/100g dm). Yellow berry percentage positively and significantly affected the TPC, TFC, and YPC contents due to the hard separation of the outer layers from the starchy grain during the debranning step.

The aim of this work is to study the effect of heat treatment on the lipidic profile of sunflower seed oil. It determined and compared the contents of bioactive components in seed oils extracted with n-hexane (Soxhlet method) from raw and roasted sunflower. The influence of torrefaction on fatty acid composition, triglyceride composition, and peroxide value (PV) has been studied. Thermal oxidation assays were carried out, and samples were evaluated by measuring induction time. Oleic acid was the main unsaturated fatty acid. Concerning triglyceride composition, OOL + LnOO, OOO + PoPP, POP and OOO + PoPP, OOL + LnOO, POP were the main, respectively, for raw and roasted samples. The seed oil samples extracted from the roasted sample exhibited a higher peroxide value (213.68 meq.O2/kg) than the raw sample (5.79 meq.O2/kg). The acid values were, respectively, 3.24 and 1.81 mg of KOH/g of oil for roasted and raw samples. On the other hand, induction time for raw sample was higher (16.23 h) than the roasted sample one (2.67 h).