The evolution of the microstructure and texture in body-centered cubic (BCC) niobium (Nb) during conventional rolling and high-ratio differential rolling (HRDSR) at room temperature were compared. More effective grain refinement of the initial microstructure through continuous dynamic recrystallization (CDRX) occurred in the samples processed by HRDSR, but the overall degree of grain refinement was small, despite having undergone severe plastic deformation due to the low rate of CDRX. CDRX more preferentially proceeded on {111} γ-fiber grains than on {001} α-fiber grains. The HRDSR-processed samples exhibited weaker α-fiber and stronger γ-fiber than the conventionally processed samples, which indicates that the high shear deformation induced by HRDSR discourages the development of α-fiber while promoting the development of γ-fiber. The HRDSR processed Nb showed a high tensile strength of 450 MPa, and the major strengthening mechanism for the HRDSR-processed Nb was dislocation-density strengthening at large thickness reductions.

In this study, Mg+B wires were prepared by powder in tube method using Nb and Cu tubes as barrier and sheath, respectively, followed by cold drawing. Microstructural, textural, and mechanical properties of the Nb barrier at different drawing strains (ε _d) were investigated. The results showed that the Nb barrier demonstrated a saturation hardness of 159.4 HV. The microstructure of the Nb barrier became elongated along the drawing direction increasing ε _d. Sub-grains existing inside the deformed grains rotated from low-angle grain boundaries to high-angle grain boundaries and developed into new grains. The main textural components of the Nb barrier were {111} γ-fiber and {hkl}〈110 〉 α-fiber. Recrystallized grains exhibited a low maximum orientation distribution function intensity, weak {100}〈110 〉 α-fibers, and strong {111}〈110 〉 γ-fibers as compared to those of the deformed grains. The relationship between the microstructure evolution and mechanical properties of the Nb barrier and the changes in the cross-sectional area fractions of the materials constituting the Mg+B composite wire are discussed. The current study provides details about the misorientation profile inside deformed grains and continuous dynamic recrystallization mechanism of the cold-drawn Nb barrier.