Microstructure has significant effects on the mechanical properties of AlSi10Mg alloy. Therefore, an in-depth understanding of microstructure evolution, such as dendrite and Al-Si eutectic, is of great significance to obtain the desirable microstructure and manage the performance of AlSi10Mg components. In the current work, an integrated dendrite and eutectic evolution model based on the cellular automaton–finite difference (CA-FD) method, taking account of solute distribution, growth kinetics, and nucleation mechanism, was established. Microstructures of the as-built selective laser melted (SLMed) samples were characterized by optical microscopy (OM), scanning electron microscopy (SEM) and electron backscatter diffraction (EBSD) techniques, and the experimental results showed that the microstructure consisted of Al grains and Al-Si eutectic networks in the individual melt pool. Dendrite growth, solute redistribution in ternary alloy and dendritic morphologies with different cooling rates were numerically investigated. In addition, the proposed model was also applied to predict the Al-Si eutectic evolution, and eutectic morphologies under eutectic undercooling in a range of 5 K to 20 K were also simulated. The simulated results indicated that dendrites were refined with the increasing of the cooling rates, and Al-Si eutectic morphology was sensitive to eutectic undercooling such that higher eutectic undercooling refined the eutectic microstructures. Model validations were performed, and the experimental results agreed well with the simulation results, indicating that the proposed model can successfully reproduce both dendrite and eutectic microstructures.
The microstructure and precipitate evolution of as-cast Mg–Nd alloys with different contents of Nd was investigated via experimental and simulation methods. The research showed that the as-cast microstructure of Mg–Nd alloy consisted of α-Mg dendrites and the intermetallic phases. A metastable β phase precipitated, followed by α-Mg dendrites that could be confirmed as Mg12Nd by X-ray diffraction (XRD) analysis. The amount of β-Mg12Nd presented a rising trend with increasing Nd additions. In addition, the tertiary phase was also observed in as-cast Mg–Nd alloy when Nd content was greater than 3 wt.%, which precipitated from the oversaturated α-Mg matrix. The tertiary phase should be β1-Mg3Nd, which is also a metastable phase with a face-centered cubic lattice. However, it is a pity that the tertiary phase was not detected by the XRD technique. Moreover, an effective cellular automaton (CA) model was explored and applied to simulate the time-dependent α-Mg/β1-Mg3Nd eutectic growth. The simulated results of α-Mg/β1-Mg3Nd eutectic growth in Mg-3Nd presented that the growth of α-Mg dendrites was accompanied by the nucleation and growth of β1-Mg3Nd precipitates and eventually formed a eutectic structure. The eutectic morphologies for Mg–Nd system alloys with different Nd contents were also simulated using the proposed model, and the results revealed that α-Mg dendrite was a refinement, and the amount of α-Mg/β1-Mg3Nd eutectic was promoted, with increasing Nd content.
The effect of the hot oscillatory pressing (HOPing) temperature on the microstructure and tensile behavior of the powder metallurgy superalloys was investigated and compared with those of the hot pressed (HPed) sample. The results show that as the HOPing temperature rises, the pores and residual dendrites disappear, the grain size becomes coarser and more uniform, the prior particle boundaries (PPBs) scale decreases; the yield strength decreases gradually; the ultimate tensile strength and elongation increase first and then decrease; the tensile property stability gradually increases. The highest ultimate tensile strength and elongation of 1403 MPa and 35%, respectively, are reached when the HOPing temperature is 1160 °C. The fracture mode of the sample hot oscillatory pressed (HOPed) at 1160 °C is a transgranular and intergranular mixed fracture. Compared with the HPed sample, room temperature tensile properties of the HOPed sample improve remarkably due to the reduced size and density of PPBs precipitates.
In the aerospace field, the BT25y titanium alloy is recommended as a candidate material for manufacturing compressor discs and rotor blades of aircraft engines. The influence of hot deformation parameters on the microstructural evolution, recrystallization softening, and globularization mechanism of the BT25y alloy with an initial lamellar structure was studied. Furthermore, the coupling relationship between dynamic recrystallization and lamellar globularization was explored by means of EBSD, SEM, and TEM techniques. The experiment results indicate that the characteristics of initial lamellar α, α/α sub-grain boundaries within α lamellae, and the α/β phase boundary show significant variations due to the formation of equiaxed α grains during hot deformation. As the strain rate increases, the recrystallization mechanism of α phase gradually shifts from CDRX softening characterized by sub-grain evolution and lamellae fracture, to DDRX softening characterized by grain boundary arching and sub-grain boundary bridging. As the deformation temperature increases, the intense thermal activation promotes the accumulation of distortion storage energy, providing enhanced driving force for the occurrence of dynamic recrystallization. The research results will contribute to a deeper understanding of the relationship between dynamic recrystallization and lamellar globularization, providing theoretical guidance for the deformation process optimization and mechanical property control of the BT25y alloy.