The microstructure and micro-mechanics around the repaired interface, and the tensile properties of laser additive repaired (LARed) Inconel 625 alloy were investigated. The results showed that the microstructure around the repaired interface was divided into three zones: the substrate zone (SZ), the heat-affected zone (HAZ), and the repaired zone (RZ). The microstructure of the SZ had a typical equiaxed crystal structure, displaying simultaneously precipitated block-shaped MC-type carbides (NbC, TiC), with bimodal sizes of approximately 10 μm and 0.5 μm and an irregularly shaped flocculent Laves phase. Recrystallization occurred in the HAZ, and led to significant grain growth; a portion of the second phase dissolved in the original grain boundaries. In the RZ, there was a columnar crystal structure, and the size increased with increasing deposition thickness. Moreover, the microstructure between the layer interface and layer interior was quite different, presenting an overlapping transition zone (OTZ), in which the dendritic structure coarsened and more Laves phase were precipitated, compared to in the layer interior. The hardness and tensile properties of the LARed samples were equivalent to those of the wrought substrate, which indicates that laser additive repairing (LAR) is a reliable repair solution for damaged and mis-machined components comprising Inconel 625 alloy.
The microstructure and precipitate evolution of as-cast Mg–Nd alloys with different contents of Nd was investigated via experimental and simulation methods. The research showed that the as-cast microstructure of Mg–Nd alloy consisted of α-Mg dendrites and the intermetallic phases. A metastable β phase precipitated, followed by α-Mg dendrites that could be confirmed as Mg12Nd by X-ray diffraction (XRD) analysis. The amount of β-Mg12Nd presented a rising trend with increasing Nd additions. In addition, the tertiary phase was also observed in as-cast Mg–Nd alloy when Nd content was greater than 3 wt.%, which precipitated from the oversaturated α-Mg matrix. The tertiary phase should be β1-Mg3Nd, which is also a metastable phase with a face-centered cubic lattice. However, it is a pity that the tertiary phase was not detected by the XRD technique. Moreover, an effective cellular automaton (CA) model was explored and applied to simulate the time-dependent α-Mg/β1-Mg3Nd eutectic growth. The simulated results of α-Mg/β1-Mg3Nd eutectic growth in Mg-3Nd presented that the growth of α-Mg dendrites was accompanied by the nucleation and growth of β1-Mg3Nd precipitates and eventually formed a eutectic structure. The eutectic morphologies for Mg–Nd system alloys with different Nd contents were also simulated using the proposed model, and the results revealed that α-Mg dendrite was a refinement, and the amount of α-Mg/β1-Mg3Nd eutectic was promoted, with increasing Nd content.
1. Beryllium-aluminum (Be-Al) alloy (with a Be content of 62 wt.%) combines the advantages of beryllium, such as low density, high specific stiffness, with the good workability of metallic aluminum...