The microstructural peculiarities of Nb powder and Nb + Al powder mixtures after mechanical activation in a high-energy planetary ball mill were investigated by transmission electron microscopy. The materials revealed two-level structural states: nanograins of size from 50 to 100 nm that contain subgrains of size ∼20 nm and less with low-angle misorientation boundaries, elastic lattice curvature gC _ij ≈100°…200°μm⁻¹, curl or curvature gradient ∂χ _ij /∂ _r > 100 μm⁻² and high (up to 10E μm⁻¹) local stress gradients (couples). An important factor in the formation of the above states is the capability of nano-objects to reach high elastic lattice curvature, high gradients of this curvature, and high local internal stress gradients at rather low absolute values of the internal stress.

The evolution of the defect substructure in V-4Ti-4Cr alloy under its severe plastic deformation by torsion in Bridgman anvils is studied by transmission electron microscopy. Nanoband structural states with a dipole or multipole character of misorientations and a crystallite (or nanoband) size varying from several to several tens of nanometers form in the true logarithmic strain range e ≈ 3.0−6.6. Such crystallites form inside 100-nm submicrocrystallites or coalesce (at e ≥ 6) to yield mesobands with a pronounced vortex character of their propagation. The formation of these states is related to the activation (by the flows of nonequilibrium point defects in stress fields) of quasi-viscous deformation and lattice reorientation mechanisms, which provide the generation and propagation of partial disclination nanodipoles followed by the development of collective effects in a disclination substructure. These effects lead to the group motion of nanodipoles inside the mesobands.

In this paper, the structural characteristics of a W-Ta-Mo-Nb-V-Cr-Zr-Ti non-equiatomic refractory metal alloy obtained by spark plasma sintering (SPS) of a high-energy ball-milled powder mixture are reported. High-energy ball milling resulted in the formation of particle agglomerates ranging from several tens to several hundreds of micrometers. These agglomerates were composed of micrometer and submicrometer particles. It was found that, during ball milling, a solid solution of A2 structure formed. The grains of the sintered material ranged from fractions of a micrometer to several micrometers. During SPS, the phase transformations in the alloy led to the formation of a Laves phase of C15 structure and ZrO and ZrO₂ nanoparticles. The microhardness of the ball-milled alloy and sintered material was found to be 9.28 GPa ± 1.31 GPa and 8.95 GPa ± 0.42 GPa, respectively. The influence of the processing conditions on the structure, phase composition, and microhardness of the alloy is discussed.

The evolution peculiarities of grain and defect structures in nickel under high-pressure torsion were studied by transmission electron microscopy and X-ray diffraction analysis. Lattice reorientation mechanisms characteristic of different stages of plastic deformation were disclosed. The conditions and features of cooperative realization of various structure formation mechanisms under severe deformation were discussed.

The paper studies the effect of the annealing temperature on microstructural transformation and micro-hardness variation in an internally oxidized vanadium alloy V—Cr—ZrO2deformed by high-pressure...