This work aims to study the possibility of obtaining Al–C composite from AlSi10MgCu aluminum matrix with the addition of 500 nm-sized diamond particles by selective laser melting (SLM) process. Al–C composite powder was prepared by mechanical mixing to form a uniform cover along the surface of aluminum particles. The diamond content in the resulting AlSi10MgCu-diamond composite powder was equal to 0.67 wt %. The selection of the optimal SLM parameters for the obtained composite material is presented. For materials characterization, the following methods were used: scanning electron microscopy (SEM), transmission electron microscopy (TEM), X-ray diffraction (XRD), and Raman spectroscopy. X-ray photoelectron spectroscopy (XPS) was applied after SLM printing for a detailed investigation of the obtained composites. The presence of carbon additives and the formation of aluminum carbides in the material after the SLM process were demonstrated.
1 March 2020 in Russian Journal of Non-Ferrous Metals
The process of deposition of allotropic modifications of carbon from the gas phase (5 vol % methane) with the use of microwave plasma on W wire 20 μm thick has been studied. The microwave power was changed in the range from 3 to 5 kW. The investigations of the structure of coatings, as well as the results of Raman spectroscopy, made it possible to establish that a microwave power of 3 kW results in the deposition of a diamond film with a crystallite size from 1 to 5 μm, microwave power of 4 kW causes the deposition of diamond-like carbon, and an increase in power up to 5 kW leads to the deposition of multigraphene film.
1 July 2017 in Refractories and Industrial Ceramics
Представлен первый этап отработки методики создания тонких покрытий карбида гафния на поверхности углерод-углеродного композиционного материала (УУКМ) при относительно небольших температурах синтеза для снижения возникающих термических напряжений. Исследован процесс образования карбида гафния на поверхности УУКМ в системе HfCl4‒СH4‒Ar при 1050 °С и атмосферном давлении. Изучена скорость процесса сублимации хлорида гафния (IV) при различных расходах газаносителя. Построены гистограммы распределения частиц карбида гафния по размерам, в результате чего установлено полидисперсное распределение частиц на поверхности УУКМ с двумя максимумами по средним диаметрам 5,4 мкм и 295 нм.
1 January 2020 in Refractories and Industrial Ceramics