In recent years significant advances have been made in the field of multiphase steels for automotive applications. Complex steel grades have been developed with exceptional mechanical properties: they combine high strength values with an excellent ductility. Transformation-induced plasticity (TRIP) steels show these properties pre-eminently. The high ductility makes TRIP steels well suited for use in energy-absorbing devices. To guarantee a controlled dissipation of the energy released during a crash, knowledge and understanding of the impact-dynamic material properties are essential. An extensive experimental programme to investigate the strain rate dependent mechanical properties was set up, and the results for two CMnAl TRIP steels and a CMnSi TRIP steel are presented in this paper. A split Hopkinson tensile bar set-up was used for the experiments. Microstructural observation techniques were used to reveal the mechanisms governing the observed high strain rate behaviour. From the results it is clear that the excellent mechanical properties not only are preserved at higher strain rates but even improve. Several phenomenological material models were investigated to describe the strain rate and temperature dependent behaviour of TRIP steels. Both the Johnson—Cook model and an extended version of the Ludwig model were found to give good agreement with the experimental data.
The 9Ni martensitic steels have a martensitic microstructure which contains retained austenite after solution heat treatment and water quenching. Under low cycle fatigue, extrusions formed at the surface of the material and were very close to martensite lath boundaries. The presence of retained austenite at martensite laths has been highly suspected to impact the cyclic plasticity. However, the nano-size of the austenitic phase makes it difficult to obtain clear evidence of its role. The paper focuses on the precise determination of these extrusions and the link with the retained austenite. The paper also emphasizes the innovative and promising use of magnetic force microscopy (MFM) to document cyclic plasticity of a 9Ni steel. It is shown that electron microscopies, even the most advanced ones, may be unsuccessful in reaching this goal, while magnetic force microscopy (MFM) overcame the difficulty. This technique has allowed imaging of both the extrusion and the retained austenite. These analyses confirm that the fatigue extrusions originated from a local displacement of martensite lath. The proposed mechanism, in which the retained austenitic film acts as a lubricant film or greasy film promoting a flowing of martensite along the interfaces, is unambiguously demonstrated.
The paper aims at documenting the material employed in 1942 for the fabrication of an exhaust valve for a Harley-Davidson WLA/WLC motorcycle and assesses the material features with modern steel standard specifications and treatment. Facing properties of the original historical parts of technical heritage objects according to modern standards is a rare discipline, as these objects are nowadays in collections of museums or private collectors and experimental instrumental analyses are strictly forbidden. In this case, a preserved accessible unused surplus replacement kit was studied. The microstructure was assessed by light optical and scanning electron microscopy, electron probe micro-analysis and by heat treatment–hardness correlation. It was found that the valve was made of Silchrome 1 steel in coherence with the X45CrSi9-3 steel modern material standard, but with a slightly higher content of phosphorus and sulfur. Microscopic observations and hardness profile testing suggested a tempered martensitic structure (sorbite) with very fine grains uniformly distributed in the valve and an even heat treatment. Heat treatment–hardness experimentation demonstrated that the original heat treatment cannot be achieved by the modern standard procedure. The tempering temperature was surprisingly deduced to be lower than the recommended one according to the modern standard, which contrasts with the service temperature indicated in the contemporary motorcycle mechanics handbook.