A developing energy-saving approach of cold sintering in a pure aqueous medium was applied to the preparation of α-Al₂O₃ ceramics and performed on spark plasma sintering equipment. The initial γ-Al(OH)₃ and γ-AlOOH powders and the cold-sintered ceramics were studied by X-ray diffraction analysis, infrared spectroscopy, thermal analysis, and scanning electron microscopy to reveal the chemical and structural transformations they experienced during the cold sintering. At 450 °C and 70 MPa, initially γ-AlOOH transformed into a fragile α-Al₂O₃ material. Porous α-Al₂O₃ ceramics with about 60% porosity were obtained after cold sintering of γ-Al(OH)₃ in the same conditions combined with subsequent annealing at 1250 °C for 3 h. The role of water molecules in the studied processes was considered as the enhancement of structural mobility in the cold-sintered material due to its reversible hydroxylation similar to earlier investigated supercritical water actions on the precursors during α-Al₂O₃ formation. Further improvement of the cold sintering setup and regimens would open prospects in α-Al₂O₃ ceramics manufacturing by an ecologically benign route.

The deformation behavior of duplex stainless steel under tension and bending, accompanied by a pulsed current and when heated by an external source, is investigated. The stress–strain curves are compared at the same temperatures. The contribution to the decrease in flow stresses is greater when using a multi-pulse current at the same temperature, compared to external heating. This confirms the presence of an electroplastic effect. An increase in the strain rate by an order of magnitude reduces the contribution of the electroplastic effect from single pulses to the reduction in flow stresses by 20%. An increase in the strain rate by an order of magnitude reduces the contribution of the electroplastic effect from single pulses to the reduction in flow stresses by 20%. However, in the case of a multi-pulse current, the strain rate effect is not observed. Introducing a multi-pulse current during bending reduces the bending strength by a factor of two and the springback angle to 6.5.

The electroplastic effect (EPE) is a phenomenon which consists in a decrease in the strain resistance and enhancing of the plasticity of metals under the effect of the electric current of a sufficiently high density [1].   The goal of the study is to compare the deformation behavior of single-phase commercially pure tita­nium Grade 4 and two-phase VT6 alloy under tension and external heating with introduction of a pulsed current. Current of various pulse ratio and density was supplied to the grips of the tensile testing machine from a pulse generator. To estimate the relative contribution of the electroplastic effect during passage of current to the reduction of flow stresses, the materials were also exposed to external heating. The microstructure of the samples in the sample head and in the vicinity of the fracture region in the longitu­dinal section was studied using optical microscopy. The electroplastic effect in the studied materials is manifested on the tensile curve through individual jumps in the downward flow stress at a high pulse ra­tio, whereas at a low current pulse ratio a decrease in the flow stress and strain hardening and increase in the plasticity are observed. It is shown that tension of the sample under the effect of current results in a greater decrease in the flow stresses than that observed under external heating at the same temperature for both materials. This confirms the athermal nature of the pulsed current effect. The critical density of the high pulse ratio current (q - 5000) capable of providing manifestation of the electroplastic effect is two times lower for a VT6 alloy than for pure titanium Grade 4. Under the same pulsed current modes, the flow stresses for VT6 decrease more than for Grade 4. Pulsed current of high pulse ratio caused an anomalous hardening effect in a VT6 alloy, but the physical nature of this effect requires an additional study. The pulsed current modes used in the study did not lead to any structural changes noticeable under optical magnification in the samples under tension, except for the disappearance of twins and separation of the impurity particles in Grade 4 and spheroidization of grains in VT6.

The characteristics of friction and wear during low-frequency reciprocating motion of the indenter in commercially pure titanium with coarse and fine grains are investigated. The role of the microstructure refining and the ratio of grain size and displacement amplitude is shown.