Additive manufacturing is a key enabling technology in the manufacture of highly complex shapes, having very few geometric limitations compared to traditional manufacturing processes. The present paper aims at investigating mechanical properties at cryogenic temperatures for a 316L austenitic stainless steel, due to the wide possible cryogenic applications such as liquid gas confinement or superconductors. The starting powders have been processed by laser powder bed fusion (LPBF) and tested in the as-built conditions and after stress relieving treatments. Mechanical properties at 298, 77 and 4.2 K from tensile testing are presented together with fracture surfaces investigated by field emission scanning electron microscopy. The results show that high tensile strength at cryogenic temperature is characteristic for all samples, with ultimate tensile strength as high as 1246 MPa at 4.2 K and 55% maximum total elongation at 77 K. This study can constitute a solid basis for investigating 316L components by LPBF for specific applications in cryogenic conditions.
Additive manufacturing, including laser powder bed fusion, offers possibilities for the production of materials with properties comparable to conventional technologies. The main aim of this paper is to describe the specific microstructure of 316L stainless steel prepared using additive manufacturing. The as-built state and the material after heat treatment (solution annealing at 1050 °C and 60 min soaking time, followed by artificial aging at 700 °C and 3000 min soaking time) were analyzed. A static tensile test at ambient temperature, 77 K, and 8 K was performed to evaluate the mechanical properties. The characteristics of the specific microstructure were examined using optical microscopy, scanning electron microscopy, and transmission electron microscopy. The stainless steel 316L prepared using laser powder bed fusion consisted of a hierarchical austenitic microstructure, with a grain size of 25 µm as-built up to 35 µm after heat treatment. The grains predominantly contained fine 300–700 nm subgrains with a cellular structure. It was concluded that after the selected heat treatment there was a significant reduction in dislocations. An increase in precipitates was observed after heat treatment, from the original amount of approximately 20 nm to 150 nm.
The article deals with increasing the mechanical properties of stainless steel 316 Ln-IG, which is intended for work in cryogenic temperatures (liquid nitrogen and liquid helium), such as conductor conduits for the ITER magnet system. The strength and plastic properties were increased by a combination of cold and cryo-rolling and heat treatment. The mechanical properties of rolled material were investigated at 293 K, 77 K, and 4.2 K. The work-hardening rate of the steel increased continuously with a lowering of the temperature. The maximum yield strength and ultimate tensile strength were achieved by the cryo-rolling process with a total thickness deformation of 50%. The material properties tested at ambient temperature were 0.2YS = 1050 MPa, UTS = 1200 MPa, and at 4.2 K, the values were 0.2YS = 1804 MPa and UTS = 2081 MPa. Two types of long-term heat treatment were applied after experimental rolling (823 K and 1093 K for 10 h). The highest precipitation hardening of steel was achieved at a temperature of 823 K after 50% deformation. The resulting grain size decreased from the initial 216 μm (before the rolling process) to 70 μm after ambient rolling and 72 μm after cryo-rolling.
The wear and degradation of tools applied in the high-pressure die casting of Al alloys induce significant financial losses. The formation of failures on the surface of mold parts caused by erosion, thermal fatigue, corrosion, and soldering negatively affects the surface quality of castings. In this study, the lifetime of inserts protected by physical-vapor-deposited coatings (TiN, TiAlN, and CrAlSiN) is examined under real manufacturing conditions while considering requirements for the castings’ surface quality (maximum average roughness Ra) defined by the customer. The goal was to identify the most suitable solution for HPDC in the foundry organization. After the deposition of PVD coatings on the inserts, the hardness (HRC) values increased from two to five depending on the coating used, and also the surface roughness was higher in the case of all inserts (Ra values increased from 0.24 to 0.36 µm). The lifetime of all PVD-coated inserts was higher compared to the uncoated insert. The highest lifetime was achieved by the application of a TiN coating, when 15,000 shots were achieved until the inserts’ wear negatively affected (increased) the surface roughness of castings, considering the customer requirements for the maximum Ra value. SEM analysis was used to identify examples of wear and degradation on the surface of the TiN coated insert.
28 February 2022 in Archives of Metallurgy and Materials
The main aim of the present paper is to evaluate the porosity and mechanical properties of Ti6Al4V and CoCrW alloys produced by Laser Powder Bed Fusion (L-PBF) as an additive manufacturing (AM) technology. Ti6Al4V and CoCrW alloys are attractive for medical application. The complex examination of porosity for these alloys needs the quantification of morphological and dimensional characteristics. Quantification of porosity was realized on non-etched samples. Quantitative image analysis was used to describe the dimensional and morphological porosity characteristics. The pores were evaluated by Image pro plus software. The results show the significant inhomogeneity of the morphology and distribution, as well as the pore size in the investigated materials and underline the importance of pore structure for the controlling mechanism of the mechanical response.