The effect of heating rate on the formation and decomposition of austenite was investigated on cold-rolled low carbon steel. Experiments were performed at two heating rates, 150 °C/s and 1500 °C/s, respectively. The microstructures were characterized by means of scanning electron microscopy (SEM) and electron backscattered diffraction (EBSD). Experimental evidence of nucleation of austenite in α/θ, as well as in α/α boundaries is analyzed from the thermodynamic point of view. The increase in the heating rates from 150 °C/s to 1500 °C/s has an impact on the morphology of austenite in the intercritical range. The effect of heating rate on the austenite formation mechanism is analyzed combining thermodynamic calculations and experimental data. The results provide indirect evidence of a transition in the mechanism of austenite formation, from carbon diffusion control to interface control mode. The resulting microstructure after the application of ultrafast heating rates is complex and consists of a mixture of ferrite with different morphologies, undissolved cementite, martensite, and retained austenite.

This work is focused on the effect of pouring temperature on the thermal-microstructural response of an eutectic spheroidal graphite cast iron (SGCI). To this end, experiments as well as numerical simulations were carried out. Solidification tests in a wedge-like part were cast at two different pouring temperatures. Five specific locations exhibiting distinct cooling rates along the sample were chosen for temperature measurements and metallographic analysis to obtain the number and size of graphite nodules at the end of the process. The numerical simulations were performed using a multinodular-based model. Reasonably good numerical-experimental agreements were obtained for both the cooling curves and the graphite nodule counts.