As a powerful numerical analysis tool, PFC (Particle Flow Code) is widely applied to investigate the mechanical behavior of rock specimen or rock engineering under different stress states. To match the macroscopic properties of the PFC model with those of the rock, a set of micro-scale parameters of the model needs to be calibrated. Thus, this paper proposed an optimization method combining Box–Behnken experimental design and desirability function approach to quickly and accurately find the values of the micro-scale parameters. The sensitivity of the main micro-scale parameters (mean value of parallel-bond normal strength σ_c, ratio of particle normal to shear stiffness E_c, and Young’s modulus at each particle–particle contact k_n/k_s) and their interactions to the macroscopic responses (uniaxial compressive strength, Young’s modulus, and Poisson’s ratio) were thoroughly analyzed using response surface theory. After that, validation study was conducted on the calibrated model. The results manifest that the uniaxial compressive strength is extremely significantly affected by σ_c and k_n/k_s, the Young’s modulus is highly correlated with E_c and k_n/k_s, and the Poisson’s ratio is most significantly influenced by k_n/k_s. Additionally, the interaction of micro-scale parameters also has different impact upon the responses. Moreover, the simulated crack behavior around differently shaped openings in rock samples under uniaxial compression is found to be well agreeable with the experimental results, which verifies the reliability of the proposed method.

The precipitation of calcium carbonate induced by Sporosarcina pasteurii (S. pasteurii) has garnered considerable attention as a novel rock and soil reinforcement technique. The content and structure of calcium carbonate produced through this reaction play a crucial role in determining the rocks’ and soil’s reinforcement effects in the later stages. Different potential gradients were introduced during the bacterial culture process to enhance the performance of the cementation and mineralization reactions of the bacterial solution to investigate the effects of electrification on the physical and chemical characteristics, such as the growth and reproduction of S. pasteurii. The results demonstrate that the concentration, activity, and number of viable bacteria of S. pasteurii were substantially enhanced under an electric field, particularly the weak electric field generated by 0.5 V/cm. The increased number of bacteria provides more nucleation sites for calcium carbonate deposition. Moreover, as the urease activity increased, the calcium carbonate content generated under an electric potential gradient of 0.5 V/cm surpassed that of other potential gradient groups. The growth rate increased by 9.78% compared to the calcium carbonate induced without electrification. Significantly, the suitable electric field enhances the crystal morphology of calcium carbonate and augments its quantity, thereby offering a novel approach for utilizing MICP in enhancing soil strength, controlling water pollution, and mitigating seepage. These findings elevate the applicability of microbial mineralization in engineering practices.

In order to improve the effect of microbial-induced calcium carbonate precipitation (MICP) in tailings reinforcement, sodium citrate, an organic matrix with good water solubility, was selected as the crystal form adjustment template for inducing calcium carbonate crystallization, and the reinforcements of tailings by MICP were conducted in several experiments. The effects of sodium citrate on the yield, crystal form, crystal appearance, and distribution of calcium carbonate were analyzed by MICP solution test; thus, the related results were obtained. These showed that the addition of a proper amount of organic matrix sodium citrate could result in an increment in the yield of calcium carbonate. The growth rate of calcium carbonate reached 22.6% under the optimum amount of sodium citrate, and the crystals of calcium carbonate were diverse and closely arranged. Based on this, the MICP reinforcement test of tailings was carried out under the action of the optimum amount of sodium citrate. The microscopic analysis using CT and other means showed that the calcium carbonate is distributed more uniformly in tailings, and the porosity of samples is significantly reduced by layered scanning analysis. The results of triaxial shear tests showed that adding organic matrix sodium citrate effectively increased the cohesion, internal friction angle, and peak stress of the reinforced tailings. It aims to provide a novel idea, a creative approach, and a method to enhance the reinforcement effect of tailings and green solidification technology in the mining environment.

Many underground reservoirs for storing water have been constructed in China’s western coal mines to protect water resources. Coal pillars which work as dams are subjected to a long-term soaking environment of concentrated salty water. Deterioration of the coal dam under the attack of the salty solution poses challenges for the long-term stability and serviceability of underground reservoirs. The evolution of the physical and mechanical properties of coal subjected to salty solutions are investigated in this paper. Coal from a western China mine is made to standard cylinder samples. The salty solution is prepared according to chemical tests of water in the mine. The coal samples soaked in the salty solution for different periods are tested by scanning electron microscope, nuclear magnetic resonance, and ultrasonic detector techniques. Further, uniaxial compression tests are carried out on the coal specimens. The evolutions of porosity, mass, microstructures of coal, solution pH values, and stress–strain curves are obtained for different soaking times. Moreover, a damage constitutive model for the coal samples is developed by introducing a chemical-stress coupling damage variable. The result shows that the corrosion effect of salty solution on coal samples becomes stronger with increasing immersion time. The degree of deterioration of the longitudinal wave velocity (v_p) is positively correlated with the immersion time. With the increase in soaking times, the porosity of coal gradually increases. The relative mass firstly displays an increasing trend and then decreases with time. The peak strength and elastic modulus of coal decreases exponentially with soaking times. The developed damage constitutive model can well describe the stress–strain behavior of coal subjected to salty solution under the uniaxial compression.

The instability and failure of coal pillars is one of the important factors leading to the catastrophic consequences of coal mine goaf collapse. Coal mine water has the characteristics of high salinity. Long-term mine water erosion can easily deform the coal pillar structure, eventually leading to instability and damage. This study carried out tests on coal samples soaked in salt solutions with different concentrations, and the nuclear magnetic resonance (NMR) method was used to obtain the dynamic evolution of the pore-fracture structure of coal. On the basis of fractal theory, the changes in fractal dimension of pore structure during the soaking process were discussed. The damage variable based on the pore fractal dimension was defined and the evolution relationship between the damage variable and immersion time was characterized. The findings demonstrated that the porosity change rate has an exponentially increasing relationship with the immersion time, and with the increasement of concentration of salt solution, the porosity change rate also shows increasing trends. The number of seepage pores and total pores increased with the immersion time. While, with the extension of soaking time, the number of adsorption pores first increased and then decreased. The connectivity between pores was enhanced. The relationship between the fractal dimension and the immersion time is linearly decreasing. The damage variable showed an increasing trend with the immersion time. As the concentration of salt solution increased, the damage of coal increased. The research results are of great significance for rationally evaluating the stability of coal pillars and ensuring the safe operation of underground engineering.

The governance of uranium tailings aims to improve stability and reduce radionuclide uranium release. In order to achieve this goal, the uranium removal solution test and uranium tailings grouting test were successively carried out using microbially induced calcium carbonate precipitation (MICP) technology. The effect of MICP on the reinforcement of uranium tailings and the synchronous control of radionuclide uranium in the tailings were discussed. The solution test results show that Sporosarcina pasteurii could grow and reproduce rapidly in an acidic medium with an initial pH of 5. The uranium concentration decreased with the increase in MICP reaction time, and the removal efficiency reached 60.9% at 24 h. In the solidification test of tailings, the strength of tailings improved significantly after 12 days of reinforcement, with an increase in the cohesion of tailings by 2.937 times and an increased internal friction angle of 8.393°. The peak stress value of solidified tailings at the surrounding pressure of 50 kPa increased by 1.87 times, and the uranium concentration in the discharge fluid decreased by 76.91% compared to the blank group. This study provides valuable insights and references for safely disposing of uranium tailings.