Ferritic stainless steels are prone to grain coarsening and precipitation of chromium-rich grain boundary phases during fusion welding, which increase intergranular corrosion susceptibility. State-of-the-art techniques to overcome these challenges mainly feature heterogeneous nucleating agents with regard to grain coarsening or alternating alloy concepts as well as post-weld heat treatments as for restoration of intergranular corrosion resistance. The present investigation seeks to depart from these traditional approaches through the use of a tailored heat input during pulsed laser beam welding by means of free-form pulse shaping. Grain size analysis using electron backscatter diffraction shows a substantial reduction of grain size as compared to continuous-wave lasers due to a distinctive columnar to equiaxed transition. Moreover, phase analyses reveal the overcoming of chromium carbide precipitation within the heat-affected zone. As corrosion tests demonstrate, intergranular attack is therefore concentrated on the weld metal. In comparison to continuous-wave laser beam welding, intergranular corrosion susceptibility is substantially reduced for very short pulse durations. From these results, it can be derived that pulsed laser beam welding using free-form pulse shaping enables direct control of heat input and, thus, tailored grain growth and precipitation formation properties.
In the present investigation, thin sheet geometries of commercially pure titanium (cp, grade 4) are butt-welded to AISI 316L stainless steel as well as Nitinol by means of micro electron beam welding using filler materials. In order to avoid mixing of the base materials, the refractory metals tantalum, niobium and hafnium are applied as intermediate layers. Owing to the biocompatibility of these filler materials, the final products are suitable for medical technology applications. In combination with low energy inputs and precise beam alignments, it is demonstrated that high-quality and crack-free joints can be produced using micro electron beam welding. The welded joints are analysed using nanoindentation to identify critical weld areas, e.g. high concentrations of intermetallic compounds, and to evaluate the compatibility of the base and filler materials. To correlate the hardness mappings with the microstructural evolution of the welds, an exemplary joint is analysed by means of electron backscatter diffraction and energy dispersive X-ray spectroscopy with special emphasis on intermixing and the formation of intermetallic compounds. Based on the generated hardness mappings as well as the ultimate tensile strengths of the joints, it will be concluded which filler material provides the most promising results for the given material combinations.
17 November 2023 in Metallurgical and Materials Transactions A
Joining of NiTi shape memory alloys with commercially pure titanium (Ti) is of great interest for manifold industrial applications. However, dissimilar fusion welding of these materials is associated with the formation of extremely brittle intermetallic compounds, e.g., Ti2Ni and TiNi3, which drastically limit the mechanical properties of NiTi/Ti joints. The present investigation seeks to improve both chemical compatibility and mechanical performance through intermixing of a niobium foil as filler material into a NiTi/Nb/Ti butt-joint configuration by means of pulsed laser beam welding. Different pulse durations are applied to tailor intermixing and evaluate the deviating chemical compositions of the weld metal. It is demonstrated that intermixing of niobium significantly increases the weldability of the material combination NiTi/Ti compared to autogenous welding. However, the proportion of intermixed filler material exerts a substantial impact on the microstructural evolution and mechanical properties. Ultimate tensile strengths of up to 679 MPa with fracture occurring in the titanium base metal at an elongation at break of 18.7 pct is obtained by a reduction of the pulse duration, which represents a major improvement over previous studies focusing on fusion welding of NiTi to titanium and its alloys.
High-speed friction stir welding (HSFSW) has emerged as a promising technique for improving the manufacturing efficiency of aluminum alloy structures by enabling faster welding while maintaining the quality of welded joints. This study investigates the mechanical properties and microstructural characteristics of AA 7020-T651 aluminum alloy joints welded using a novel multi-pin tool at high feed rates ranging from 2500 to 6000 mm/min under a constant rotational speed of 4000 rpm. Defect-free welds were successfully fabricated, as confirmed by metallographic analysis and micro-computed tomography (µ-CT). The multi-pin tool facilitated consistent material flow and heat distribution, which contributed to reliable joint formation across all feed rates. At the highest feed rate, the tensile strength reached 76% of the base material. A consistent softening in the nugget zone (NZ) was observed, and electron backscatter diffraction (EBSD) analysis showed a more than 70% grain size reduction in this zone, averaging ~3 µm, due to dynamic recrystallization. These findings underscore the suitability of HSFSW with multi-pin tools for high-speed industrial applications, offering enhanced productivity without compromising structural integrity.
The present study focuses on the weldability of hot-rolled Fe–Mn–Al–Ni shape memory alloy sheets by vacuum electron beam welding. Tailored process-specific welding parameters, such as preheating with electron beam or beam oscillation during welding, allowed defect-free joining with very thin weld seams and heat-affected zones. By applying a post-weld cyclic heat treatment, abnormal grain growth can be promoted across the weld seams. However, regardless of the selected welding parameters, some specimens are characterized by the formation of smaller grains within the former fusion zone. In situ incremental strain tests reveal that the former fusion zone has only a minor influence on the functional properties and is not responsible for structural failure. Thus, electron beam welding is a promising welding technology for joining Fe–Mn–Al–Ni shape memory alloys.
In the present investigation, commercially pure titanium is welded to AISI 316L stainless steel by intermixing niobium as filler material in a lap joint configuration. For this purpose, a pulsed Nd:YAG laser with various pulse durations and pulse peak powers is employed to obtain different mixing conditions for the materials. It will be demonstrated that, despite the implementation of the filler material, the weld seams are characterized by a high affinity for cracking, which in turn can be attributed to the formation of hard intermetallic compounds. Nevertheless, utilization of optimized process parameters can yield crack-free specimens in a reproducible manner through equable intermixing of otherwise critical alloy elements. Lap-shear forces of up to 140 N can be achieved with a single weld seam measuring 2.5 mm in length. By increasing the joint area with four adjacent weld seams, maximum loads up to 320 N are attained, thus exceeding the yield strength of the applied stainless steel. Considering the biocompatibility of the niobium filler material used, this work provides the foundation for this dissimilar material combination to be implemented in future medical technology applications.