Considering persistent years, many researchers continuously seek an optimum way to utilize the idea of magnetorheology (MR) materials to be practically used for everyday life, particularly concerning resistivity sensing application. The rheology and resistivity of a graphite (Gr)-based magnetorheological elastomer (Gr-MRE) were experimentally evaluated in the present research. Magnetorheological elastomer (MRE) samples were prepared by adding Gr as a new additive during MRE fabrication. The effect of additional Gr on the rheological and resistivity properties were investigated and compared with those of typical MREs without a Gr additive. Morphological aspects of Gr-MRE were characterized using field emission scanning electron microscopy (FESEM) and energy dispersive X-ray spectroscopy (EDX). Rheological properties under different magnetic fields were evaluated using a parallel-plate rheometer. Subsequently, the resistivity of all samples was measured under different applied forces and magnetic fields. From the resistivity evaluation, two relationship curves resistance (R) under different applied forces (F) and different magnetic fields (B) were established and plotted by using an empirical model. It was observed from the FESEM images that the presence of Gr fractions arrangement contributes to the conductivity of MRE. It was also observed that, with the addition of Gr, rheological properties such as the field-dependent modulus can be improved, particularly at low strain amplitudes. It is also demonstrated that the addition of Gr in MRE can contribute to the likely use of force detection in tactile sensing devices.
The effect of different types of multiwall carbon nanotubes (MWCNTs) on the morphological, magnetic and viscoelastic properties of magnetorheological elastomers (MREs) are studied in this work. A series of natural rubber MRE are prepared by adding MWCNTs as a new additive in MRE. Effects of functionalized MWCNT namely carboxylated MWCNT (COOH-MWCNT) and hydroxylated MWCNT (OH-MWCNT) on the rheological properties of MREs are investigated and the pristine MWCNTs is referred as a control. Epoxidised palm oil (EPO) is used as a medium to disperse carbonyl iron particle (CIP) and sonicate the MWCNTs. Morphological and magnetic properties of MREs are characterized by field emission scanning electron microscopy (FESEM) and vibrating sample magnetometer (VSM), respectively. Rheological properties under different magnetic field are evaluated by using parallel plate rheometer. From the results obtained, FESEM images indicate that COOH-MWCNT and CIP have better compatibility which leads to the formation of interconnected network in the matrix. In addition, by adding functionalized COOH-MWCNT, it is shown that the saturation magnetization is 5% higher than the pristine MWCNTs. It is also found that with the addition of COOH-MWCNT, the magnetic properties are improved parallel with enhancement of MR effect particularly at low strain amplitude. It is finally shown that the use of EPO also can contribute to the enhancement of MR performance.
The existing mold concept of fabricating magnetorheological elastomer (MRE) tends to encounter several flux issues due to magnetic flux losses inside the chamber. Therefore, this paper presents a new approach for enhancing particle alignment through MRE fabrication as a means to provide better rheological properties. A closed-loop mold, which is essentially a fully guided magnetic field inside the chamber, was designed in order to strengthen the magnetic flux during the curing process with the help of silicone oil (SO) plasticizers. The oil serves the purpose of softening the matrix. Scanning electron microscopy (SEM) was used to observe the surface morphology of the fabricated MRE samples. The field-dependent dynamic properties of the MREs were measured several ways using a rheometer, namely, strain sweep, frequency sweep, and magnetic field sweep. The analysis implied that the effectiveness of the MRE was associated with the use of the SO, and the closed-loop mold helped enhance the absolute modulus up to 0.8 MPa. The relative magnetorheological (MR) effects exhibited high values up to 646%. The high modulus properties offered by the MRE with SO are believed to be potentially useful in industry applications, particularly as vibration absorbers, which require a high range of stiffness.
This paper investigates the field-dependent rheological properties of magnetorheological (MR) fluid used to fill in MR dampers after long-term cyclic operation. For testing purposes, a meandering MR valve was customized to create a double-ended MR damper in which MR fluid flowed inside the valve due to the magnetic flux density. The test was conducted for 170,000 cycles using a fatigue dynamic testing machine which has 20 mm of stroke length and 0.4 Hz of frequency. Firstly, the damping force was investigated as the number of operating cycles increased. Secondly, the change in viscosity of the MR fluid was identified as in-use thickening (IUT). Finally, the morphological observation of MR particles was undertaken before and after the long-term operation. From these tests, it was demonstrated that the damping force increased as the number of operating cycles increases, both when the damper is turn on (on-state) and off (off-state). It is also observed that the particle size and shape changed due to the long operation, showing irregular particles.