This report describes a new approach to successfully synthesize high-quality nickel oxide (NiO) nanorods with an average diameter of about 60 nm and a length of less than one micrometre viathermal decomposition of a precursor complex nickel benzoate dihydrazinate at 100 °C. The structural features, crystallinity, purity and morphology of the as-synthesized NiO nanorods were investigated by Raman spectroscopy, X-ray diffraction (XRD), scanning electron microscopy (SEM), selected area electron diffraction (SAED) and transmission electron microscopy (TEM). The electrochemical property of the as-synthesized NiO nanorods was investigated to determine their suitability as anode materials for lithium-ion batteries. The nanorod electrode exhibited better reversibility and high capacity. In addition, the nanorods showed good antibacterial properties. The magnetic measurement demonstrated that the NiO nanorods are ferromagnetic and may be used in the fields of MR imaging and magnetic drug delivery.
1 January 2013 in International Journal of Photoenergy
Chitosan (CS) anchored copper oxide (CuO) hybrid material was prepared by chemical precipitation method. Fourier transform infrared spectroscopy (FT-IR) and X-ray diffraction (XRD) confirmed the formation of CS-CuO hybrid. Transmission electron microscopy (TEM) analysis showed the immobilization of CuO nanoparticles on the surface of CS. The hybrid was also characterized by thermogravimetric analysis (TGA) and zeta potential. The hybrid exhibited high photocatalytic activity as evident from the degradation of methylene blue (MB) dye. The result revealed substantial degradation of the MB dye (84%) under UV-light illumination. The antibacterial activity of hybrid againstEscherichia coliwas examined by colony forming units. It was proved that the CS encapsulated CuO hybrid exhibited excellent antibacterial activity.