This study presents the experimental results of fresh and hardened properties of concrete incorporating high-volume fly ash (HVFA). Two kinds of low-calcium fly ash with loss on ignition (LOI) of 5% and 8% were used as replacement for cement and/or fine aggregate of 0% (control), 20%, 40%, 50%, 60% and 80% by weight of the total cementitious materials. The properties of fresh concrete tested included the slump, air content, unit weight and setting time; those of hardened concrete determined included compressive strength, modulus of elasticity, flexural strength and drying shrinkage. Test results indicate that the concretes made with high-LOI (8%) fly ash can be successfully produced for structural concrete, which contains fly ash of up to 60% of the total cementitious materials. The high-LOI fly ash-concretes with higher replacement levels presented longer setting times. However, although both the fresh and hardened properties of high LOI fly ash concretes were inferior to those of the low-LOI (5%) fly ash concretes, the high modulus of elasticity, the adequate strength development characteristics both at early and later ages (up to 365 days) and the low dry shrinkage were observed when compared to those of the control concrete with a comparable 28-day compressive strength of 30 MPa.

This study aimed to apply the Taguchi optimization technique to determine the process conditions for producing synthetic lightweight aggregate (LWA) by incorporating tile grinding sludge powder with reservoir sediments. An orthogonal array L₁₆(4⁵) was adopted, which consisted of five controllable four-level factors (i.e., sludge content, preheat temperature, preheat time, sintering temperature, and sintering time). Moreover, the analysis of variance method was used to explore the effects of the experimental factors on the particle density, water absorption, bloating ratio, and loss on ignition of the produced LWA. Overall, the produced aggregates had particle densities ranging from 0.43 to 2.1 g/cm³ and water absorption ranging from 0.6% to 13.4%. These values are comparable to the requirements for ordinary and high-performance LWAs. The results indicated that it is considerably feasible to produce high-performance LWA by incorporating tile grinding sludge with reservoir sediments.

To investigate potential implications of microbial activity on sand bioconsolidation and subsurface environments, two ureolytic strains, Sporosarcina pasteurii and Bacillus subtilis were tested for the production of calcium carbonate (CaCO₃). Laboratory experiments with monoculture S. pasteurii (column 1) and coculture S. pasteurii-B. subtilis (column 2) were conducted to determine urea and calcium chloride reactivity and volumetric carbonate formation. Both columns were able to consolidate sand, whereas, column 1 induced greater CaCO₃ precipitation. X-ray diffraction (XRD) and scanning electron microscopy (SEM) showed two columns with different mineralogy with calcite, and vaterite formation. Column 1 showed rhombohedral and trigonal crystals morphology, whereas column 2 developed the prismatic calcite and the spherulite vaterite crystals might be due to the differences of the micro-environment caused by the urease expression of these bacterial species. These results indicate the possibility of using those crystals to cement loose sand whereas, highlighted the importance of combining these techniques to understand the geomicrobiology found in the subsurface environments.

This report describes a novel way to generate a highly effective hydrophobic cement surface via a carbonation route using sodium stearate. Carbonation reaction was carried out at different temperatures to investigate the hydrophobicity and morphology of the calcium carbonate formed with this process. With increasing temperatures, the particles changed from irregular shapes to more uniform rod-like structures and then aggregated to form a plate-like formation. The contact angle against water was found to increase with increasing temperature; after 90 °C there was no further increase. The maximum contact angle of 129° was obtained at the temperature of 60 °C. It was also found that carbonation increased the micro hardness of the cement material. The micro hardness was found to be dependent on the morphology of the CaCO₃ particles. The rod like structures which caused increased mineral filler produced a material with enhanced strength. The ¹³C cross polarization magic-angle spinning NMR spectra gave plausible explanation of the interaction of organic-inorganic moieties.

The lightweight aggregates used by the civil engineering market are sintered at a high temperature, about 1200 °C. In times of high energy prices and regulation of carbon dioxide emissions, lightweight aggregate products of the high-temperature process in sales marketing are not readily accepted. This study developed a sintered-type paper sludge lightweight aggregate. In order to reduce energy consumption, substitution of some reservoir sediment clay in paper sludge substitutes is to be expected. The study used two types of paper sludge (green clay paper sludge and paper pulp sludge). The sintering temperature was reduced effectively as the green clay paper sludge was substituted for some of the reservoir sediment clay, and the optimum substitute ranges of green clay paper sludge were 10%–50%. The optimum substitute ranges of the paper pulp sludge were 10%–40%. Test results show that the properties of aggregates have a particle density of 0.66–1.69 g/cm³, a water absorption of 5%–30%, and a loss on ignition of 10%–43%. The loss on ignition of aggregate became greater with the increase in paper sludge content. This means that the calorific value provided by the paper sludge will increase as paper sludge content increases. Paper sludge can therefore be considered a good material to provide heat energy for sintering lightweight aggregate.

Self-consolidating lightweight aggregate concrete (SCLC) is a highly flowable and lightweight concrete. In this study, the properties of SCLC and prestressed SCLC members were tested and compared with those made of normal-weight self-consolidating concrete (SCC). The test results show that SCLC can be used for prestressed concrete members. The use of lightweight aggregates with a particle density larger than 1100 kg/m³ can avoid the serious segregation of fresh concrete. In addition, the SCLC designed in this study can meet most of the SCC Rank 2 test standards, except for the V-funnel test. The water contained in the lightweight aggregates supplied sustained curing, so the level of drying shrinkage of the SCLC was lower than that of the conventional SCC. However, the level of creep of the SCLC was higher than that of the conventional SCC, because normal-weight aggregates are more able to inhibit the change of the concrete’s volume. On-site test results show that after 180 days of prestressing, the prestress loss was about 5.35–6.83% for the full-size SCLC members, which was smaller than that for the conventional SCC members (about 8.19–9.06% loss).