In this study, the influence of the technological parameters of autoclave curing on the resulting mechanical properties of laminates was investigated. The main criterion for optimizing the curing was to extend the processing window with a lower prepreg viscosity. At the same time, the issue of setting the pressure level before the heat ramp to the final cure temperature was also addressed. An experimental method of measuring the indentation viscosity of the prepreg was used to determine the viscosity profile. Despite the experimental nature of the method, the reliability of this method for rapid approximate identification of the processing window of the prepreg was verified by the results of the study. Several laminates with the same ply orientation were produced using the selected cure cycles, from which test specimens were cut with a water jet and inspected by confocal microscopy. The mechanical properties of tension and flexure were measured within the individual curing cycles using tests according to ISO standards. The data reported demonstrate that the experimental method of optimizing the curing parameters has successfully increased the selected mechanical properties. The resulting mechanical properties of the laminates were enhanced by up to 20% compared to the non-optimized cure cycle. The influence of the type of cure cycle on the resulting thickness of the cured laminate was evaluated in this study.
The presented study focuses on measuring volume changes in elastomeric materials using digital image correlation (DIC), specifically the 2D DIC universal system and the 2D DIC video-extensometer directly implemented to the universal testing machine. Optical measurement methods were applied in twodimensional (2D) configurations during the mechanical testing of dumbbell-shaped test specimens under uniaxial tension. The measured data were used to determine the dependencies of the bulk modulus and Poisson's ratio on the strain. The dependencies obtained by both methods correspond to the model behavior of rubber-like materials. Compared to the 2D DIC implemented video-extensometer, the 2D DIC universal system provides a tool for measuring transverse and longitudinal strain, and a wide range of post-processing options, including change of the input parameters, settings, or calculation relations.
An equibiaxial tension test could be necessary to set up hyperelastic material constants for elastomers exactly. Unfortunately, very often, only uniaxial tension experimental data are available. It is possible to use only uniaxial data to compute hyperelastic constants for a hyperelastic model, but the prediction of behavior in different deformation modes (as is equibiaxial or pure shear) will not work correctly with this model. It is quite obvious that there is some relation between uniaxial and equibiaxial behavior for the elastomers. Thus, we could use uniaxial data to predict equibiaxial behavior. If we were able to predict (at least approximately) equibiaxial data, then we could create a hyperelastic model usable for the general prediction of any deformation mode of elastomer. The method of the appropriate processing of experimental data for such prediction is described in the article and is verified by the comparison with the experiment. The presented results include uniaxial and equibiaxial experimental data, the created average curve of both the deformation modes, and the predicted equibiaxial data. Using Student’s t-test, a close coincidence of the real and predicted equibiaxial data was confirmed.
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12 October 2023 in Acta Polytechnica CTU Proceedings
The presented research aims at measuring the volume changes of elastomers using digital image correlation (DIC) in the 3D configuration (stereo DIC). The deformation measurement method in stereo configuration was applied during the mechanical testing of two types of test specimens (dumbbells, cylinders) in uniaxial tension. In this configuration, two cameras were used. The test specimens were measured up to a specified strain value, and the measured data were used to obtain the strain dependence of Poisson’s ratio and the bulk modulus, which are crucial for hyperelastic models. The measurement results reveal that the stereo DIC method provides relatively less scattered data in the low-strain regions for dumbbell-shaped test specimens and is suitable for measuring various test specimen shapes.