The oxidation behavior of Ni–9.5Co–(8~12)Cr–(2.5~5.5)Mo–(4~8)W–3Al–5Ti–3Ta–0.1C–0.01B alloys was investigated at 850 °C and 1000 °C The mass change, the phase of oxides, and the cross-sectional structure of specimens were analyzed after cyclic oxidation tests. The oxide scale was composed mainly of Cr₂O₃ and NiCr₂O₄, but NiO, TiO₂, and CrTaO₄ were also found. Al₂O₃ was formed beneath the Cr oxide layer. The Cr oxide layer and internal Al oxide acted as barriers to oxidation at 850 °C, while Al oxide was predominantly protective at 1000 °C. Cr increased the mass gain after oxidation test at both temperatures. Mo increased the oxidation rate at 850 °C but decreased the oxidation rate at 1000 °C. W slightly increased the mass gain at 850 °C but did not produce a significant effect at 1000 °C. The effects of Cr, Mo, W, and the temperature were discussed as well as the volatilization of oxides, the valence number of elements, and diffusion retardation.

A compositional approach to designing alloys that have an enlarged equiaxed zone is suggested in this study. The partitioning of elements during the solidification of CoCrFeMnNi high-entropy alloy (HEA) was confirmed through a directional solidification quenching experiment. Several HEAs were designed to maximize the effects of constitutional and thermal undercooling by considering factors including solute enrichment at the columnar front and the melting temperatures and thermal conductivities of the individual elements. The newly designed HEAs were shown to have successfully enlarged equiaxed zones, and improved anisotropic properties.

This study investigated the microstructural evolution of the weld interface and creep fracture behavior of 10% Cr martensitic steel welds using Haynes 282 filler metal. The welded joints were subjected to post-weld heat treatment (PWHT) at temperatures of 738 °C for 4, 8, and 15 h. Creep tests were carried out at 600 °C under stress of 200 MPa. The creep rupture life increased with an increase in holding time for PWHT up to 8 h compared to the as-welded condition. However, when the holding time for PWHT was further increased to 15 h, creep properties (i.e., rupture life and creep strain) decreased considerably, and the failure location was found to shift from the ICHAZ to the weld interface. The microstructural investigation revealed that Type I carbides precipitated at the weld interface and recrystallized grains with Cr depletion were formed near Type I carbides in the partially mixed zone during creep exposure. The creep failure at the weld interface began on the surface and propagated inward through the recrystallized grains of the weld-interface region.

The efficiency of gas turbines depends on the gas turbine working temperature. Single crystal blades are being applied more often than equiaxed blades in gas turbine engines, to increase the turbine inlet temperature, resulting in enhanced turbine engine efficiency. Single crystal blades endure creep conditions at high temperature better than polycrystal blades because the single crystals do not include grain boundaries. The single crystal process is a breakthrough technology, however, production yield is relatively low compared with polycrystal, and their mechanical properties depend on the crystallographic orientation of the single crystals. In this study, a thermal simulation model, the 3D cellular automation-finite element (CA-FE), was used on the single crystal process with the Bridgman method. The simulation model was well expected, by analysis of the microstructure and EBSD, on the grain selection in the single crystal process. The evolution of single crystal grains was analyzed on process of grain selection in start block and spiral selector. Single crystal orientation was also investigated to determine the effect of nucleation density, forming in the initial stage of solidification.