Near-infrared spectroscopic (NIR) technique was used, for the first time, to predict volatile phenols content, namely guaiacol, 4-methyl-guaiacol, eugenol, syringol, 4-methyl-syringol and 4-allyl-syringol, of aged wine spirits (AWS). This study aimed to develop calibration models for the volatile phenol’s quantification in AWS, by NIR, faster and without sample preparation. Partial least square regression (PLS-R) models were developed with NIR spectra in the near-IR region (12,500–4000 cm⁻¹) and those obtained from GC-FID quantification after liquid-liquid extraction. In the PLS-R developed method, cross-validation with 50% of the samples along a validation test set with 50% of the remaining samples. The final calibration was performed with 100% of the data. PLS-R models with a good accuracy were obtained for guaiacol (r² = 96.34; RPD = 5.23), 4-methyl-guaiacol (r² = 96.1; RPD = 5.07), eugenol (r² = 96.06; RPD = 5.04), syringol (r² = 97.32; RPD = 6.11), 4-methyl-syringol (r² = 95.79; RPD = 4.88) and 4-allyl-syringol (r² = 95.97; RPD = 4.98). These results reveal that NIR is a valuable technique for the quality control of wine spirits and to predict the volatile phenols content, which contributes to the sensory quality of the spirit beverages.

The purpose of this work is to evaluate the wine spirit aged by an alternative process (staves combined with different micro-oxygenation levels) and its comparison with the traditional process (wooden barrels). This evaluation was made by analyzing the volatile compounds and sensory profile of the spirits during 365 days of ageing. The findings confirmed the role played by oxygen in the volatile profile of aged wine spirits. Samples of alternative ageing modalities were well distinguished from those of wooden barrels based on the volatile profile, namely on the concentrations of several volatile phenols. From a sensory point of view, the results are promising with high overall consistency scores obtained from samples of alternative ageing process modalities.

Macroalgae are rich in bioactive compounds with potential therapeutic applications, including antioxidant, antimicrobial, and nutritional properties. In this study, the biochemical composition of three seaweed species—Ulva sp., Gracilaria multipartita, and Sargassum muticum—was analysed, focusing on their mineral content and macronutrient profile. The ash, protein, fibre, lipid, and carbohydrate contents ranged from (dw) 26.56 to 33.53 g/100 g, 10.13 to 18.43 g/100 g, 0.11 to 0.19 g/100 g, 5.83 to 10.88 g/100 g, and 42.48 to 53.27 g/100 g, respectively. The findings indicate that the species studied are excellent sources of essential minerals, particularly magnesium, potassium, calcium, sodium, and trace elements, such as iron, zinc, copper, and manganese. Sargassum muticum exhibited the highest mineral content and thus holds significant promise for further exploration in biomedical and therapeutic contexts. FTIR, FT-RAMAN, and FT-NIR analysis highlight the presence of proteins, lipids, carbohydrates, including cell wall phycocolloids, and phenolic compounds. These results underscore the potential of macroalgae as natural sources of bioactive compounds for health-related applications, highlighting their value beyond traditional dietary supplementation.

In ancient times, the shoots of certain species within the Cytisus genus were used as animal feed. Cytisus striatus is a plentiful and widespread shrub that has long been utilized as a soil fertilizer in the Iberian Peninsula. The flowers of this shrub have traditionally been employed for medicinal purposes. However, the nutritional value of yellow broom flowers and fruits remains largely unexplored. In this study, flowers and fruit of C. striatus (Cytisus striatus) were collected from natural shrubs at three different locations in Portugal during the same year. An analytical assessment of their macro and micronutrient content was conducted. Regarding nutritional composition, flowers and fruits exhibited a fibre content of 18% and 42%, protein content of 21% and 12%, lipid content of 2% and 1%, carbohydrate content of 43% and 14%, and ash content of 4% and 3%, respectively. Potassium was the most abundant mineral, with concentrations of approximately 20,094 mg/kg in the flowers and 11,746 mg/kg in the fruits, followed by calcium, phosphorus, and magnesium. Compared to some edible flowers and fruits, these plant parts of C. striatus showed macro and micronutrient values similar to species such as lavender, lupins, and cowpea pod husks.