Coarse primary and eutectic Mg₂Si phases were generally precipitated in Mg-Al-Si alloys during solidification at a low cooling rate, which tends to deteriorate the strength and ductility of magnesium alloys due to stress concentration. Different volume fractions of TiB₂ nanoparticles (1%, 3%, and 5%) were added to an Mg-4Al-1.5Si alloy to refine the coarse Mg₂Si phases based on a heterogeneous nucleation mechanism. The nanoparticles were incorporated and dispersed in the molten Mg alloys and by using semi-solid stirring followed by ultrasonic treatment (SSUT), and TiB₂/Mg-4Al-1.5Si composites were obtained. The effect of TiB₂ content on the microstructure and mechanical properties of the composites was studied. The results showed that the average size of primary Mg₂Si phases and α-Mg grains decreased as the TiB₂ content raised, the dendritic primary Mg₂Si phases were refined into polygonal shapes with smaller sizes, and the refined primary Mg₂Si phases were uniformly distributed in the alloys after adding 1 vol.% or 3 vol.% TiB₂ nanoparticles. As the TiB₂ content increased, the morphology of the eutectic Mg₂Si phases was modified from coarse Chinese characters to short rod or fine dot shapes. Vickers hardness and yield strength of the composites reached a maximum (153 HV and 90.9 MPa, respectively) when TiB₂ content was 5 vol.%, while the most superior ultimate tensile strength (142.4 MPa) and elongation (9.2%) were obtained when TiB₂ content was 3 vol.%, which were improved by 173.2%, 31.5%, 69.8%, and 187.5%, respectively compared with the Mg-4Al-1.5Si alloys.

Purpose: The carbon/carbon (C/C) composite finger seal experiment was performed on a high-speed seal tester. The purpose of this paper is to investigate the leakage and wear characteristics of C/C composite finger seal under various operating conditions. Design/methodology/approach: Static, dynamic, endurance and post endurance tests were carried out. For static and performance tests, the pressure differential changed from 0.1 to 0.6 MPa and the rotor speed varied from 1,000 to 9,000 r/min. Two endurance tests were conducted for 4 h, with each mounting two finger seals. The seal leakage was monitored by mass flowmeters, and the wear depth was measured and calculated by using three-dimensional profilometer. Findings: Results showed that the seal leakage increases with pressure differential but decreases with rotor speed. Leakage rate is lower when speed is decelerated than that with the speed stepped up. During a time history, material removal caused by wear has significant influence on leakage data causing higher leakage than the results before endurance test. Particular interest is that the uneven wear characteristic on finger foot bottom was firstly revealed, showing severe wear in foot heel area than that in foot toe. Originality/value: This study could provide experimental guidance for finger seal designers. Additionally, the uneven wear characteristic of finger foot was firstly revealed, which showed the necessity of further theoretical research on finger seal wear.

Fused deposition modeling (FDM) technique is one of the most popular additive manufacturing techniques. Infill density is a critical factor influencing the mechanical properties of 3D-printed components using the FDM technique. For irregular components with variable cross-sections, to increase their overall mechanical properties while maintaining a lightweight, it is necessary to enhance the local infill density of the thin part while decreasing the infill density of the thick part. However, most current slicing software can only generate a uniform infill throughout one model to be printed and cannot adaptively create a filling structure with a varying infill density according to the dimensional variation of the cross-section. In the present study, to improve the mechanical properties of irregular components with variable cross-sections, an adaptive-density filling structure was proposed, in which Hilbert curve with the same order was used to fill each slice, i.e., the level of the Hilbert curves in each slice is the same, but the side length of the Hilbert curve decreases with the decreasing size of each slice; hence, the infill density of the smaller cross-section is greater than that of the larger cross-section. The ultimate bearing capacity of printed specimens with the adaptive-density filling structure was evaluated by quasi-static compression, three-point bending, and dynamic compression tests, and the printed specimens with uniform filling structure and the same overall infill density were tested for comparison. The results show that the maximum flexural load, the ultimate compression load, and the maximum impact resistance of the printed specimens with the adaptive-density filling structure were increased by 140%, 47%, and 82%, respectively, compared with their counterparts using the uniform filling structure.

The effects of Mn addition on the room temperature tensile strength and deformation mechanisms of as-cast Mg-8Al-1Nd-1.5Gd-xMn alloys (x = 0, 0.3, 0.5, 1.0 wt.%) are investigated in this paper. The results indicate that the addition of Mn contributes to the precipitation of Al-Mn-RE intermetallics and the refinement of α-Mg matrices, thereby improving the tensile strength of the 1.0 Mn alloy at 190 MPa. The fracture mechanism of Mn-containing alloys transforms from a cleavage fracture to a ductile fracture as the Mn content increases from 0.3 to 1.0 wt.%. The presence of intermetallic particles in the dimples confirms the hindrance effect of Al₁₀Mn₂ (Nd,Gd) on dislocation slips. The novel technology of in-grain misorientation axes (IGMAs) is used to identify activated slip modes and deformation twins. It can be concluded that the activated pyramidal <a> slip during tensile deformation significantly promotes the ductility of the 1.0 Mn alloy with an elongation rate of 9.8%. It is worth noting that reducing the coarse $\left\{10\overline{1}2\right\}$ tensile twins and enhancing the proportion of $\left\{10\overline{1}1\right\}$ compressive twins and $\left\{10\overline{1}1\right\}$-$\left\{10\overline{1}2\right\}$ double twins contributes to maintaining the continuous plastic deformation of Mg alloy.

Ni-CNTs/AZ91 magnesium matrix composites were fabricated by ultrasound treatment combined with a semi-solid stirred method for the first time. The agglomerated spherical Ni-CNTs transferred from spherical shape to clear tubular shape after pre-dispersion treatment. For the Ni-CNTs/AZ91 magnesium matrix composite prepared by semi-solid stirring followed by ultrasonic treatment, Ni-CNTs were evenly distributed in the magnesium matrix or wrapped on the β (Mg₁₇Al₁₂) phase. Mg₂Ni were formed at the interface of the magnesium matrix and CNTs by in-situ reaction, which significantly improved the interface bonding strength of CNTs and the Mg matrix. The tensile strength and elongation of 1.0wt.% Ni-CNTs/AZ91 magnesium matrix composites were improved by 36% and 86%, respectively, compared with those of AZ91 matrix alloy. After Ni-CNTs were added to AZ91 matrix alloy, more dimples were observed at the fracture surface. The fracture behavior of Ni-CNTs/AZ91 composite was transformed from a cleavage fracture of AZ91 matrix alloy to a quasi-cleavage fracture. Meanwhile, the CNTs dispersed near the fracture showed a “pull-out” state, which would effectively bear and transfer loads. The strengthening mechanism of CNTs was also discussed.