The paper aimed to study the evolution of the microstructure and texture gradient of a 321-type metastable austenitic stainless steel during cold rotary swaging. Cold rotary swaging was carried out with a reduction of up to 90% at ambient temperature. Pronounced gradients of the α’-martensite volume fraction, the axial texture of austenite (⟨111⟩ and ⟨001⟩) and α’-martensite (⟨101⟩), and non-uniform microhardness distribution along the rod diameter were obtained after a reduction of 80–90%. According to the finite element analysis, moderate tensile stresses were attained in the center, whereas high compressive stresses operated at the edge. Due to water cooling of the rod surface and heating of the rod center during processing, a temperature gradient was also derived. Features of strain-induced martensitic transformation, microstructure and texture evolution, and non-uniform hardening during cold rotary swaging were discussed.
The microstructure, texture, and mechanical properties of Inconel 718 fabricated via hybrid wire-arc additive manufacturing (WAAM) with inter-pass forging, and the subsequent modified post-deposition heat treatment (PDHT), were investigated. The modified PDHT included homogenization at 1185 °C and double ageing at 720 °C, with furnace-cooling to 620 °C; this process was first used for Inconel 718 obtained via WAAM and inter-pass forging. In the as-printed material, two characteristic zones were distinguished, as follows: (i) columnar grains with a preferable orientation and (ii) fine grains with a random crystallographic orientation. The development of static recrystallization induced via inter-pass forging and further heating during the deposition of the next (upper) layer provoked the formation of the fine-grained zone. In the as-printed material, particles of (Nb,Ti)C and TiN, and precipitates of a Nb-rich Laves phase that caused premature cracking and failure during mechanical testing, were detected. In the PDHT material, two zones were found, as follows: (i) a zone with coarse uniaxial grains and (ii) a zone with a gradient grain size distribution. PDHT resulted in the precipitation of γ″ nanoparticles in the γ-Ni matrix and the dissolution of the brittle Laves phase. Therefore, significant hardening and strengthening, as well as increases in ductility and impact toughness, occurred.
The present study aimed to discover the effect of cold swaging reduction on the bulk gradient structure formation and mechanical properties of a 316-type austenitic stainless steel. The initial rod was subjected to radial swaging until 20–95% reduction of initial rod diameter, at room temperature. According to finite element simulation, higher plastic strain was accumulated in the surface layer compared to the center region during swaging. Microstructural investigations revealed three-stage gradient structure formation in the center and edge regions of the deformed rod. Meanwhile, cold swaging resulted in the development of strong 111ǁBA, 001ǁBA, and weak 111ǁBA texture components in the center and edge, respectively. Significant tensile strengthening was observed after cold swaging. For instance, the yield strength (YS) increased from 820 MPa to 930 MPa after 40–80% reduction respectively, without the loss of ductility (δ–14%). This unique aspect of the mechanical behavior was attributed to the gradient structure of the cold swaged material and explained in detail.
31 January 2025 in Materials Science and Engineering: A
Slag bases for welding materials have been developed from mineral raw materials and man–made mineral formations of the Urals. Successful comprehensive studies and tests of fused fluxes and also of weld metal and weld joints obtained by these welding materials have been carried out. It has been clearly established that the obtained weld metal has low content of harmful impurities ([S] is as low as 0.01 wt%) due to the use of the electric arc furnace method, purity of the feedstock minerals and technogenic raw materials and physicochemical reactions during the welding process.