Grain refinement is of very important significance for improving the microstructure and mechanical properties of Mg alloys. This work investigated how the addition of various amounts of Y element affected the microstructure and mechanical properties of Mg-9Al-1Zn alloy. It was found that the grain size of Mg-9Al-1Zn alloy decreases as Y element content increases. When 1.2 wt.% Y element content was added, the grain size of Mg-9Al-1Zn alloy could be reduced from 334.2 μm to 134.6 μm, and grain refinement efficiency of 60% was achieved. HRTEM analysis demonstrated a good orientation relationship between the Al2Y phase and the Mg interface, and therefore, it was determined that the Al2Y phase can be used as a heterogeneous nucleation site for α-Mg grains, which promotes the grain refinement of α-Mg grain. Furthermore, the addition of Y element can also significantly refine the eutectic Mg17Al12 phase of the Mg-9Al-1Zn alloy. In this way, the mechanical properties of the Mg-9Al-1Zn alloy are significantly enhanced. It was found that the YS and UTS of the Mg-9Al-1Zn alloy reached 87 MPa and 154 MPa with the addition of 0.9 wt.% of Y element—24% and 43% higher than the Mg-9Al-1Zn alloy.
The development of lightweight composites with superior mechanical properties and electromagnetic interference (EMI) shielding performance is essential for various structural and functional applications. This study investigates the effect of hybrid nanocarbon (graphene nanosheet (GNS) and carbon nanotube (CNT)) reinforcements on the properties of magnesium (Mg) matrix composites. Specifically, the GNS-CNT hybrid, which forms a three-dimensional interconnected network structure, was analyzed and compared to composites reinforced with only GNSs or CNTs. The objective was to determine the benefits of hybrid reinforcements on the mechanical strength and EMI shielding capability of the composites. The results indicated that the GNS-CNT/Mg composite, at a nanocarbon content of 0.5 wt.% and a GNS-CNT ratio of 1:2, achieved optimal performance, with a 55% increase in tensile strength and an EMI shielding effectiveness of 70 dB. The observed enhancements can be attributed to several key mechanisms: effective load transfer, which promotes tensile twinning, along with improved impedance matching and multiple internal reflections within the GNS-CNT network, which enhance absorption loss. These significant improvements position the composite as a promising candidate for advanced applications requiring high strength, toughness, and efficient electromagnetic shielding, providing valuable insights into the design of high-performance lightweight materials.
8 July 2025 in Advanced Composites and Hybrid Materials
The development of nanoparticle-reinforced Mg matrix composites (NPMMCs) as lightweight structural materials with balanced strength and ductility remains challenging due to nanoparticle agglomeration, interfacial oxidation, and poor melt wettability. This study introduces an innovative molten salt-assisted high-temperature dispersion strategy to overcome these limitations. By employing molten salts (MgCl₂-KCl-NaCl) as dual-functional agents for anti-oxidation and thermal dispersion, we achieve uniform spatial distribution of TiC nanoparticle (TiCnp) while suppressing interfacial reactions. Meanwhile, the superiority of the high-temperature liquid medium ameliorates the wettability of TiCnp and the Mg melt. Combined with thermomechanical processing, this approach enhances interfacial bonding and activates synergistic strengthening mechanisms, yielding a 130% improvement in yield strength. The proposed methodology establishes a scalable pathway for fabricating high-performance NPMMCs, with implications for aerospace and transportation applications requiring lightweight structural components. Graphical Abstract
Magnesium alloys with a high volume fraction of secondary phases exhibit inferior formability. Therefore, investigating their thermal deformation characteristics is critical for optimizing thermal processing techniques. In this work, isothermal compression experiments were performed on a Mg-15Gd-8Y-6Al-0.3Mn alloy with an elastic modulus of 51.3 GPa with a substantial volume of aluminum-rare earth (Al2RE) phases. The rheological behavior and microstructural evolution of the material were systematically investigated at varying temperatures (350–500 °C) and strain rates (0.001–1.000 s−1). The calculated thermal processing diagram indicates that the unstable region gradually enlarges with increased strain, and all unstable regions appear within the high-strain-rate, low-temperature domain. The ideal thermal processing range of the alloy is 350–500 °C at strain rates ranging from 0.001 to 0.016 s−1. Particle-stimulated nucleation and discontinuous dynamic recrystallization are both verified to be responsible for the recrystallized microstructure of the alloy. The recrystallized grains exhibit a relatively random crystallographic orientation. As recrystallization proceeds, the texture gradually transitions from a typical [0001] texture in the compression direction to a random texture accompanied by decreased texture intensity. This work sheds new light on the thermo-mechanical processing of high-modulus Mg alloys, which could help design suitable processing techniques for related materials.
15 April 2023 in Acta Metallurgica Sinica (English Letters)
This study examined the comprehensive properties of Mg-Zn-Nd-Zr alloys in order to achieve both high strength and thermal conductivity simultaneously. The impact of rolling on the microstructure, mechanical properties, and thermal conductivity was analyzed for Mg-5Zn-xNd-0.4Zr alloys (x = 1, 2). The results indicate that the addition of Nd promotes the formation of the W phase (Mg3Zn3RE2), which contributes to grain boundary strengthening and enhances the overall strength. Moreover, dynamic precipitation during the rolling process leads to the formation of nanoscale MgZn2 and Zn2Zr phases, significantly improving both the strength and thermal conductivity. After rolling, both the Mg-5Zn-1Nd-0.4Zr (ZNK510) and Mg-5Zn-2Nd-0.4Zr (ZNK520) alloys exhibited a notable enhancement in thermal conductivity, with ZNK520 demonstrating superior properties due to its higher Nd content. This study highlights that optimizing alloy composition and phase evolution through rolling can markedly enhance both the mechanical and thermal properties, offering a promising strategy for the development of high-performance magnesium alloys.