This paper investigates how the thickness of dogbone tensile specimens made from heat-treated Hastelloy-X alloy produced by Laser Powder Bed Fusion (LPBF) influences their mechanical properties and microstructure. The focus of the investigation is on surfaces in an “as-built” condition and considers a range of thickness from 3 to 1 mm. The “as-built” surfaces condition is a fundamental outcome, considering that LPBF technology’s key feature is the ability to produce intricate and complex geometries that are difficult to achieve with conventional manufacturing technologies. The specimens were fabricated according to ASTM E8/E8M-21 and were heat-treated in a vacuum furnace at 1150 °C for two hours. The microstructure of the material was evaluated through porosity, EBSD, and Microhardness analyses. The mechanical properties were evaluated through tensile tests conducted at room temperature on dogbone specimens fabricated both parallel and perpendicular to the building direction. The findings indicate a significant reduction in mechanical properties that could be correlated with the reduction in specimen thickness, reflecting a gradual decline from the baseline. Specifically, a 14% decrease in Ultimate Tensile Strength (from 612 to 528 MPa), an approximately 19% reduction in Young’s Modulus (from 190 GPa to 153 GPa), and a 32% decrease in Elongation at Break (from 59.2% to 40.0%) were observed. Furthermore, it was noted that the printing orientation of the specimens significantly affects their mechanical properties, regardless of thickness. Overall, the results suggest that applying standard heat treatment under specific conditions, such as with a thin, exposed wall of about 1mm with a striped strategy, may not lead to adequate material performance.

Additive Manufacturing (AM) processes, particularly PBF-LB/M, are considered advantageous due to their flexibility, which allows process engineers to design and fabricate intricate structures both in the prototyping and component manufacturing phases. It is well known that the behavior of the process directly impacts the quality of the materials and thereby induces inhomogeneities on the powder bed on the building platform. Several parameters can be tuned to keep the process under control, getting rid of process uncertainty and distinguishing aspects of a specific machine model. Such behavior requires an extended analysis of the powder bed inhomogeneities and the definition of limits in the printing process. In this work, carried out on Alloy 718 specimens printed using an EOS M290 machine, the inhomogeneities of the melt pool stability, density, and material properties were investigated based on three main factors: the amount of area melted or fused, the gas flow speed setpoint, and the location on the building platform. The test results for Track Stability, melt-pool shape, and porosity analysis show that criticality occurs when more than 50% of the building platform is exposed. This can be partly fixed by raising the differential pressure value.

In the framework of high temperature components, the need to evaluate the accumulated creep damage during service life is fundamental to extend the life of components which are currently deemed as scrap as per design intent. Thus, the life assessment of Ni-based superalloys could be performed in relation to the accumulated creep deformation which represents the limiting factor for serviced components. Despite the different microstructural changes that occur in service life, this work focuses on the possibility to evaluate the material strain by means of electron backscattered diffraction (EBSD). The key point is the identification of the correlation between geometrically necessary dislocation (GND) density derived from EBSD analyses and the reached creep strain for a single crystal Ni-based superalloy. However, the results of GND density are affected by the settings’ parameters adopted to perform the analysis by the magnification level and the step size. These two parameters have been optimized by analyzing specimens from interrupted creep tests at strain levels between 0.5% and 10%, in the temperature range between 850 °C and 1000 °C.