The Al-Si cast alloy family is widely used in the production of complex castings for various applications and known for its very good castability and high strength-to-weight ratio. However, early cracking under tensile loading is sometimes a limiting factor. Among other parameters, it is yet controversial whether grain boundaries are dominant strengthening factor in cast alloys, instead of dendrite/eutectic boundaries. This study presents the effect of secondary dendrite arm spacing (SDAS) and grain size on crack initiation and propagation of Al-Si cast alloys under tensile loading. The Al-10Si (wt.%) alloy with modified Si morphology was cast using inoculants (Al-5Ti-B master alloy) under different cooling rates to obtain a range of grain sizes (from below 138 μm to above 300 μm) and SDAS (6, 15 and 35 μm). Conventional tensile test as well as in-situ tensile test in a scanning electron microscope, equipped with an electron backscatter diffraction (EBSD) was carried out to understand the deformation mechanisms of the alloy. Observation of slip bands within the dendrites showed that in modified Si structure, the interdendritic (eutectic) area takes more portion of the strain during plastic deformation. Besides, only a few cracks were initiated at the grain boundaries; they were mostly initiated from dendrite/eutectic interface. All cracks propagated trans-granularly. Hall-Petch calculations also showed a strong relationship between SDAS and flow stress of the cast alloy. Although statistically correct, there was no physically meaningful relationship between the grain size and the flow stress. Nevertheless, formation of identical slip bands in each grain could be an evidence for the marginal effect of the grain size on the overall strength development of the alloy. Consequently, among other effects, the combinational dominant effect of SDAS and modest effect of grain size shall be considered for modification of the Hall-Petch equation for precise prediction of mechanical properties of cast alloys
The effect of three important process parameters, namely laser power, scanning speed and laser stand-off distance on the deposit geometry, microstructure and segregation characteristics in direct energy deposited alloy 718 specimens has been studied. Laser power and laser stand-off distance were found to notably affect the width and depth of the deposit, while the scanning speed influenced the deposit height. An increase in specific energy conditions (between 0.5 J/mm2 and 1.0 J/mm2) increased the total area of deposit yielding varied grain morphologies and precipitation behaviors which were comprehensively analyzed. A deposit comprising three distinct zones, namely the top, middle and bottom regions, categorized based on the distinct microstructural features formed on account of variation in local solidification conditions. Nb-rich eutectics preferentially segregated in the top region of the deposit (5.4–9.6% area fraction, Af) which predominantly consisted of an equiaxed grain structure, as compared to the middle (1.5–5.7% Af) and the bottom regions (2.6–4.5% Af), where columnar dendritic morphology was observed. High scan speed was more effective in reducing the area fraction of Nb-rich phases in the top and middle regions of the deposit. The crystallographic direction was observed to be the preferred growth direction of columnar grains while equiaxed grains had a random orientation.
1 January 2022 in Materials Science and Engineering: A