: The influence of keyhole TIG (K-TIG) welding parameters on the weld geometry and defects of a new nickel-based superalloy VDM Alloy 780 alloy were investigated using a statistical design of experiment, and the microstructures of the heat-affected zone (HAZ) and fusion zone (FZ) of the K-TIG-welded VDM Alloy 780 were characterized. No cracks are found in the FZ and HAZ. Travel speed significantly influences the minimum weld width (Wm), face and root excess weld metal, face underfill, and average pore diameter. Welding current and the interaction current*travel speed significantly influence the face and root excess weld metals, respectively. Interdendritic microconstituents in the FZ are identified as (Nb,Ti)C particles and γ/Laves eutectic constituents based on SEM–EDS analysis. In addition, plate-like precipitates likely to be δ/η phase are observed surrounding the interdendritic Laves eutectics, and γ′ precipitates are found to be inhomogeneously precipitated in the FZ. In the partially melted zone (PMZ), (Nb,Ti)C, Laves phase, and plate-like particles are found in the liquated and resolidified regions. Constitutional liquation of (Nb,Ti)C in HAZ is observed where the liquated (Nb,Ti)C appears to be associated with the γ/Laves eutectic as a resolidified product.
Effective thermal management is essential in metal additive manufacturing to ensure process stability and desirable material properties. Directed energy deposition using a laser beam and wire (DED-LB/w) enables the production of large, high-performance components but remains sensitive to adverse thermal effects during multi-layer deposition due to heat accumulation. While prior studies have investigated interlayer temperature control and substrate preheating in DED modalities, including laser-powder and arc-based systems, the influence of substrate preheating in DED-LB/w has not been thoroughly examined. This study employs substrate preheating to simulate heat accumulation and assess its effects on melt pool geometry, wire–melt pool interaction, and the microstructural evolution of Alloy 718. Experimental results demonstrate that increased substrate temperatures lead to a gradual expansion of the melt pool, with a notable transition occurring beyond 400 °C. Microstructural analysis reveals that elevated preheat temperatures promote coarser secondary dendrite arm spacing and the development of wider columnar grains. Moreover, Nb-rich secondary phases, including the Laves phase, exhibit increased size but relatively unchanged area fractions. Observations from electrical conductance measurements and coaxial visual imaging show that preheat temperature significantly affects the process dynamics and microstructural evolution, providing a basis for advanced process control strategies.
27 August 2025 in Journal of Materials Research and Technology
The fusion zone microstructures in K-TIG-welded and post-weld solution heat-treated new superalloy VDM Alloy 780 were examined. In addition, the kinetics of the base metal grain growth during solution heat treatments were analyzed. (S)TEM analyses show that major interdendritic microconstituents formed in the fusion zone due to elemental microsegregation are MC carbides and coarse irregularly shaped Laves phase. Additionally, minor secondary interdendritic phases are found to include γ′, γ″, and tiny plate-like Laves particles. To prevent any potential deterioration of mechanical properties caused by the irregular Laves phase, post-weld solution heat treatments (PWSHTs) at 954 °C to 1060 °C/1 hours were performed to remove the Laves phase. PWSHT at 954 °C only partially eliminates the Laves particles while forming an abundance of interdendritic δ/η phase. Laves phase is dissolved entirely without forming δ/η platelets after PWSHT at 1060 °C. It is proven that Laves eutectics in VDM Alloy 780’s fusion zone can be eliminated through PWSHT without significantly coarsening the base metal’s grain size in comparison to Alloy 718 as a result of substantial grain growth inhibition likely caused by solute segregation at grain boundaries.