Fixed-target serial femtosecond crystallography (FT-SFX) was an important advance in crystallography by dramatically reducing sample consumption, while maintaining the benefits of SFX for obtaining crystal structures at room temperature without radiation damage. Despite a number of advantages, preparation of a sample holder for the sample delivery in FT-SFX with the use of many crystals in a single mount at ambient temperature is challenging as it can be complicated and costly, and thus, development of an efficient sample holder is essential. In this study, we introduced a nylon mesh-based sample holder enclosed by a polyimide film. This sample holder can be rapidly manufactured using a commercially available nylon mesh with pores of a desired size at a low cost without challenging technology. Furthermore, this simple device is highly efficient in data acquisition. We performed FT-SFX using a nylon mesh-based sample holder and collected over 130,000 images on a single sample holder using a 30 Hz X-ray pulse for 1.2 h. We determined the crystal structures of lysozyme and glucose isomerase using the nylon mesh at 1.65 and 1.75 Å, respectively. The nylon mesh exposed to X-rays produced very low levels of background scattering at 3.75 and 4.30 Å, which are negligible for data analysis. Our method provides a simple and rapid but highly efficient way to deliver samples for FT-SFX.
Blocking the near-infrared region (NIR) is indispensable for saving energy consumed to maintain the interior temperature in buildings. However, simultaneously enhancing transmission in visible light and blocking in the NIR remains challenging. Here, we theoretically demonstrate a transparent all-dielectric metasurface selectively blocking the NIR by using TiO2 nanocylinders and an indium tin oxide (ITO) layer. The ITO layer is implemented as a back reflector because ITO is transparent in visible light, whereas the ITO becomes a reflective material in the long-wavelength region (λ > 1500 nm). The designed metasurface exhibits high average transmittance of 70% in visible light and high solar energy rejection (SER) of 90% in the NIR. Furthermore, the blocking capability in the NIR of the designed metasurface is maintained over a wide range of an incident angle and polarization angle of light. Therefore, the metasurface gives a guideline for designing energy-saving applications.
13 August 2021 in ACS Applied Materials & Interfaces
This study presents a lightweight metasurface microwave absorption filter (MMAF) designed for low-frequency stealth applications in the L-band. The metasurface is optimized using a genetic algorithm to achieve broadband absorption at subwavelength thickness. The fabricated MMAF consists of a glass fiber-reinforced plastic layer, a metasurface layer, and a dielectric layer with a size of 30 × 30 cm2. It maintains a reflection coefficient below −10 dB in the frequency range of 1.01–1.78 GHz. Experiments using small MMAFs measuring 15 × 15 cm2 confirmed stable performance after composite molding. In addition, the results from small MMAFs configured in a 2 × 2 array were similar to those of the 30 × 30 cm2 structure. These results highlight the potential of the MMAF for scalable deployment on curved or segmented surfaces, expanding its applicability to various stealth platforms.