This study experimentally evaluates the mechanical and microstructural performance of single- and double-layer intraply hybrid composite (IRC) laminates produced using the hand lay-up method, focusing on Glass–Aramid (GA), Aramid–Carbon (AC), and Carbon–Glass (CG) configurations. Tensile, flexural, compressive, and density tests were conducted in accordance with relevant ASTM standards to assess the influence of hybrid type and layer number under field-representative manufacturing conditions. Microstructural investigations were performed using optical microscopy and scanning electron microscopy (SEM) to identify fabrication-induced imperfections and their relationship to mechanical behavior. The results demonstrate that increasing the laminate configuration from single to double layer significantly enhances mechanical performance across all hybrid types. Double-layer AC laminates exhibited the highest tensile strength (330.4 MPa) and Young’s modulus (11.93 GPa), corresponding to improvements of approximately 85% and 59%, respectively, compared to single-layer counterparts. In flexural loading, the highest strength was observed in double-layer CG laminates (97.14 MPa), while compressive strength was maximized in double-layer AC laminates (34.01 MPa), indicating improved stability and resistance to compression-driven failure. Statistical analysis confirmed that layer number is the dominant parameter governing mechanical response, exceeding the influence of hybrid configuration alone. Microstructural observations revealed fiber misorientation, incomplete resin impregnation, and localized voids inherent to manual fabrication. However, these imperfections were consistently distributed across all specimens and did not obscure comparative mechanical trends. Coefficients of variation generally remained below 10%, indicating acceptable repeatability despite non-ideal manufacturing conditions.

Polymer-based materials have become increasingly used in concrete production and various engineering applications due to their versatile properties. In particular, polymer concrete (PC) has become a preferred reinforcement material in the construction industry. Various studies have been carried out to evaluate the performance of PC and to improve its mechanical properties by adding different admixtures. This study investigates the effects of fine materials such as iron powder (IP) and blast furnace slag (BFS) on the mechanical performance of PC. Within the scope of the study, samples with 5% and 10% IP, 5% and 10% BFS, 2.5% IP + 2.5% BFS and 5% IP + 5% BFS were prepared. These specimens were cured in the same laboratory environment and subjected to mechanical tests at the end of the 7th day. The results of the mechanical tests were compared to reveal the effect of fine materials on the performance of the PC. The potential of an artificial neural network (ANN) model is investigated to replicate real-world outcomes. The findings provide valuable insights into the potential of iron powder and blast furnace slag as admixtures to improve the mechanical properties of PC.