The use of lignocellulosic remnants of the açaí agro-business will benefit the environment with a precursor material for biomedical applications. Nanocellulose (NC) allows the biomimetic growth of biphasic ceramics on its surface, with characteristics compatible with bone tissue, including bioactive properties and biocompatibility. In this study, the composites were obtained from açaí tegument (Euterpe Oleracea Mart.) NC using acid hydrolysis. The characterization performed by scanning electron microscopy showed the characteristic crystals of hydroxyapatite (HA) and calcium triphosphate (β-TCP) based on the results of X-ray diffraction, with the peak at 22°, showing the NC nucleation of HA and peak at 17° showing tricalcium phosphate (β-TCP). Fourier transform infrared spectroscopy confirmed the presence of O-H at 3400 cm⁻¹ and C-H at 2900 cm⁻¹, which is characteristic of cellulose; peaks were also observed at 1609 cm⁻¹, verifying the reduction in lignin content. Groups PO₄⁻³ at approximately 1070 cm⁻¹, P-OH at 910–1040 cm⁻¹, and HCO₃⁻ at 2450 cm⁻¹ confirmed the formation of HA and β-TCP. The zeta potential had a range of −11 ± 23.8 mV related to particle size, which had a range of 164.2 × 10⁻⁹–4748 × 10⁻⁹ m.

This work aims to evaluate the melting temperature and wetting behavior of AlN/Re₂O₃ (Re = Dy, Yb) mixtures when in contact with SiC substrates at high temperatures, in order to define whether these compounds can be further used to induce a more effective liquid phase sintering of SiC-based products. The prepared samples were placed on SiC plates and thermally treated up to 1900 °C under argon. The melting point and spreading evolution of different compositions of AlN/Re₂O₃ on SiC were determined by analyzing images captured as a function of the heating temperature. The contact angle and melting point were measured using the ImageJ software and according to DIN 51730, respectively. Based on the obtained wetting curves, all evaluated conditions resulted in the decrease of the contact angle values with temperature. The mixtures presenting improved wetting (θ ~ 1° and 3°) on SiC plates were the ones above the selected eutectic point.