“Fracture network stimulation + imbibition replacement” is a new attempt to effectively develop tight sandstone reservoirs, and the fractures provide conditions for fluid imbibition replacement. On the basis of nuclear magnetic resonance and pseudo-color processing technology, combined with the imbibition experiments, this paper studies the imbibition process of fractured tight sandstone reservoirs, clarifies the effect of each level of pore-throat on imbibition, and realizes the visualization of the imbibition process. The results show that, in fractured tight sandstone reservoirs, the fluid displacement occurs in fractures first, followed by pore-throat. Most of the imbibition recovery is contributed by the macropore, the contribution of the mesopore to imbibition recovery is very weak, and the contributions of the micropore and the pinhole are even less. In the process of imbibition, capillary force and gravitational force are key parameters controlling fluid flow in pores and fractures. The replacement of fluid normally takes place in the early stage of imbibition, especially on the first day of imbibition, then the imbibition rate gradually decreases and finally tends to be stable.
“Fracturing network+imbibition oil production” is a new attempt to effectively develop low-permeability tight reservoirs. Fracturing fluid is not only a carrier for sand carrying but also a tool in the process of imbibition. On the basis of imbibition experiments, combined with nuclear magnetic resonance and pseudo-color processing technology, this paper clarified the dominant forces of different types of pore-throat and quantitatively characterized the contribution of different levels of pore-throat to imbibition oil recovery. The results show that gravity is the main controlling force of imbibition for reservoirs with higher permeability. Fluid replacement mainly occurs in the early period of imbibition. Macropores contribute most of the imbibition recovery, mesopores have a weak contribution, and the contribution of micropores and pinholes can be ignored. For the reservoirs with low permeability, capillary force is the main controlling force of imbibition. Fluid replacement mainly occurs in the later period of imbibition. Macropores contribute most of the imbibition recovery rate, mesopores contribute a small part of the imbibition recovery factor, and the contribution of micropores and pinholes can be ignored. This paper clarified that macropores and mesopores are the main sources of the contribution of imbibition recovery efficiency, and oil content and connectivity are key factors for the imbibition recovery efficiency.
This study investigates the impact of nanomaterials on different surfactant solutions. By measuring the parameters (including emulsification property, zeta potential, DLS, CA, IFT, etc.) of imbibition liquid system with nanoparticles and without nanoparticles, combining with imbibition experiments, the law and mechanism of improving the imbibition recovery of nanomaterials were obtained. The findings demonstrate that the nano-silica sol enhances the emulsification and dispersion of crude oil in the surfactant system, resulting in smaller and more uniform particle sizes for emulsified oil droplets. Non-ionic surfactant AEO-7 has the best effect under the synergistic action of nanomaterials. Zeta potential and DLS tests also showed that AEO-7 exhibits smaller particle sizes due to their insignificant electrostatic interaction with nanoparticles. Furthermore, the addition of nanomaterials enhances the hydrophilicity of core and reduces the interfacial tension. Under the synergistic action of nanoparticles, AEO-7 still showed the best enhanced core hydrophilicity (CA 0.61° after imbibition) and the lowest interfacial tension (0.1750 mN·m−1). In the imbibition experiment, the imbibition recovery of the system with nanomaterials is higher than that of the non-nanomaterials. The mixed system of AEO-7 and nano-silica sol ZZ-1 has the highest imbibition recovery (49.27%). Combined with the experiments above, it shows that nanomaterials have a good effect on enhancing the recovery rate of tight core, and the synergistic effect of non-ionic surfactant AEO-7 with nanomaterials is the best. Moreover, nanomaterials reduce adhesion work within the system while improving spontaneous imbibition recovery. These findings provide theoretical guidance for better understanding the mechanism behind nanomaterial-induced imbibition enhancement as well as improving tight oil’s imbibition recovery.
With the exploitation of tight sandstone gas, the corrosion problem of wellbores in the X block of the Ordos Basin has become increasingly severe, necessitating the implementation of effective measures to mitigate tubing corrosion and enhance corrosion inhibition efficiency. This study conducted field corrosion monitoring in conjunction with laboratory experiments, employing weight loss method, scanning electron microscopy (SEM), energy dispersive spectroscopy (EDS), and X-ray diffraction (XRD) to comprehensively characterize the corrosion of gas wells from both macro and micro perspectives. The results show that the gas wells in the X block of the Ordos Basin are exposed to a complex corrosion environment, where the electrochemical corrosion risk in the aqueous phase and the acidic gas corrosion risk in the gas phase coexist, posing a potential threat to wellbore integrity. Corrosion in X-1 and X-2 wells is mainly attributed to CO2, while corrosion in X-3 well is primarily caused by sulfides. The field application of corrosion inhibitor M exhibited significant corrosion inhibition effects on steels, with the best performance at a dosage of 2000 mg/L. Based on experimental data, a corrosion inhibitor dosage prediction model for the X block gas wells was constructed. By increasing the dosing frequency and reducing the dosing concentration, the optimized dosing scheme can annually save approximately 566.4 L of corrosion inhibitor per well, providing a scientific basis for extending the service life of the gas well tubing. Given the prevalence of CO2- and H2S-induced corrosion in many global reservoirs, these findings provide valuable insights for corrosion management in similar international oil and gas fields, enhancing the broader applicability of the study.
“Fracture network stimulation and oil-water infiltration and replacement” are recent attempts to effectively produce oil from tight reservoirs. On the one hand, the formation can be fractured by the fracturing fluid, which can carry proppant into fractures. On the other hand, the fracturing fluid can spontaneously infiltrate into the pores under the action of capillary pressure to displace the oil phase, thereby enhancing the oil recovery. To distinguish imbibition and displacement processes during fluid replacement in tight reservoirs is difficult, and the effect of these two processes is also vaguely defined. In this study, an experimental method that can visualize the imbibition and displacement process is proposed by combining the core slice displacement experiment. Based on this method, the process of imbibition and displacement can be effectively distinguished, and imbibition retention rate can be quantitatively characterized. The effectiveness of this method is proved by taking the core of Chang 7 tight sandstone reservoir in the Ordos Basin as the research object. The results show that the force direction of the fluid under imbibition is related to the wettability, and it is always from the wetting phase to the nonwetting phase, while the force direction of fluid under displacement is mainly related to the directivity of displacement pressure difference. Based on the difference of force action, imbibition and displacement can be quantitatively characterized, respectively. During the imbibition process, the peak value of the NMR curve corresponding to the small pore throat shifts to the left, and the signal amplitude increases. During the displacement process, the peak value of the NMR curve corresponding to the small pore throat has no obvious shift, nor signal amplitude change, but the peak value of the curve corresponding to the large pore throat shifts to the right. The results also indicate that there is an exponential negative correlation between imbibition retention rate and gas permeability. The greater the gas permeability is, the smaller the imbibition retention rate is.