The exceptional performance of graphene has driven the advancement of its preparation techniques and applications. Laser-induced graphene (LIG), as a novel graphene preparation technique, has been applied in various fields. Graphene periodic structures created by the LIG technique exhibit superhydrophobic characteristics and can be used for deicing and anti-icing applications, which are significantly influenced by the laser parameters. The laser surface treatment process was simulated by a finite element software analysis (COMSOL Multiphysics) to optimize the scanning parameter range, and the linear array surface structure was subsequently fabricated by the LIG technique. The generation of graphene was confirmed by Raman spectroscopy and energy-dispersive X-ray spectroscopy. The periodic linear array structure was observed by scanning electron microscopy (SEM) and confocal laser imaging (CLSM). In addition, CLSM testings, contact angle measurements, and delayed icing experiments were systematically performed to investigate the effect of scanning speed on surface hydrophobicity. The results show that high-quality and uniform graphene can be achieved using the laser scanning speed of 125 mm/s. The periodic linear array structures can obviously increase the contact angle and suppress delayed icing. Furthermore, these structures have the enhanced ability of the electric heating deicing, which can reach 100 °C and 240 °C within 15 s and within 60 s under the DC voltage power supply ranging from 3 to 7 V, respectively. These results indicate that the LIG technique can be developed to provide an efficient, economical, and convenient approach for preparing graphene and that the hydrophobic surface array structure based on LIG has considerable potential for deicing and anti-icing applications.
There has been a significant shift in research focus in recent years toward laser-induced graphene (LIG), which is a high-performance material with immense potential for use in energy storage, ultrahydrophobic water applications, and electronic devices. In particular, LIG has demonstrated considerable potential in the field of high-precision human motion posture capture using flexible sensing materials. In this study, we investigated the surface morphology evolution and performance of LIG formed by varying the laser energy accumulation times. Further, to capture human motion posture, we evaluated the performance of highly accurate flexible wearable sensors based on LIG. The experimental results showed that the sensors prepared using LIG exhibited exceptional flexibility and mechanical performance when the laser energy accumulation was optimized three times. They exhibited remarkable attributes, such as high sensitivity (~41.4), a low detection limit (0.05%), a rapid time response (response time of ~150 ms; relaxation time of ~100 ms), and excellent response stability even after 2000 s at a strain of 1.0% or 8.0%. These findings unequivocally show that flexible wearable sensors based on LIG have significant potential for capturing human motion posture, wrist pulse rates, and eye blinking patterns. Moreover, the sensors can capture various physiological signals for pilots to provide real-time capturing.
The advancement in performance in the domain of flexible wearable strain sensors has become increasingly significant due to extensive research on laser-induced graphene (LIG). An innovative doping modification technique is required owing to the limited progress achieved by adjusting the laser parameters to enhance the LIG’s performance. By pre-treating with AgNO3, we successfully manufactured LIG with a uniform dispersion of silver nanoparticles across its surface. The experimental results for the flexible strain sensor exhibit exceptional characteristics, including low resistance (183.4 Ω), high sensitivity (426.8), a response time of approximately 150 ms, and a relaxation time of about 200 ms. Moreover, this sensor demonstrates excellent stability under various tensile strains and remarkable repeatability during cyclic tests lasting up to 8000 s. Additionally, this technique yields favorable results in finger bending and hand back stretching experiments, holding significant reference value for preserving the inherent characteristics of LIG preparation in a single-step and in situ manner.
In the rapidly advancing era of intelligent technology, flexible strain sensors are emerging as a key component in wearable electronics. Laser-induced graphene (LIG) stands out as a promising fabrication method due to its rapid processing, environmental sustainability, low cost, and superior physicochemical properties. However, the stretchability and conformability of LIG are often limited by the substrate material, hindering its application in scenarios requiring high deformation. To address this issue, we propose a high-performance flexible and stretchable strain sensor fabricated by generating graphene on a polyimide (PI) substrate using laser induction and subsequently transferred onto a polydimethylsiloxane (PDMS). The resultant sensor demonstrates an ultra-low detection limit (0.1%), a rapid response time (150 ms), a wide strain range (40%), and retains stable performance after 1000 stretching cycles. Notably, this sensor has been successfully applied to the real-time monitoring of civil aviation test pilots during flight for the first time, enabling the accurate detection of physiological signals such as pulse, hand movements, and blink frequency. This study introduces a unique and innovative solution for the real-time health monitoring of civil aviation test pilots, with significant implications for enhancing flight safety.
Flexible wearable strain sensors demonstrate promising application prospects in health monitoring, human-machine interaction, motion tracking, and the detection of human physiological signals. Although laser-induced graphene (LIG) materials have been extensively utilized in these scenarios, traditional types of LIG sensors are constrained by intrinsic limitations, including discontinuous conductive networks and electromechanical responsive hysteresis. These limitations hinder their applications in micro-strain detection scenarios. Consequently, enhancing the performance of LIG-based sensors has become a crucial priority. To address this challenge, we developed a novel MXene/LIG composite featuring optimized conductive networks and interfacial coupling effects through the systematic enhancement of LIG. The flexible strain sensor fabricated using this composite exhibits exceptional performance, including an ultra-low sheet resistance of 14.1 Ω, a high sensitivity of 20.7, a micro-strain detection limit of 0.05%, and a rapid response time of approximately 65 ms. These improvements significantly enhance electromechanical responsiveness and strain detection sensitivity. Furthermore, the sensor exhibits remarkable stability under varying tensile strains, particularly showing outstanding repeatability across 2500 cyclic tests. Notably, when applied to the pilot health monitoring scenarios, the MXene/LIG-based sensor demonstrates robust capability in detecting body movement signals such as micro-expressions and joint movements. This establishes a novel and highly effective technological solution for the real-time monitoring of pilots’ motion states during operational scenarios.
The exceptional performance of graphene has driven the advancement of its preparation technique and application. Laser-induced graphene (LIG), as a novel graphene preparation technique, has been applied in various fields. Graphene periodic structures created by LIG technique exhibit superhydrophobic characteristics and can be used for deicing and anti-icing applications, which are significantly influenced by the laser parameters. The laser surface treatment process was simulated by a finite element software analysis (COMSOL Multiphysics) to optimize the scanning parameter range, and the linear array surface structure were subsequently fabricated by the LIG technique. The generation of graphene was confirmed by Raman spectroscopy, and energy-dispersive X-ray spectroscopy. The periodic linear array structure were observed by Scanning electron microscopy (SEM) and confocal laser imaging (CLSM). In addition, CLSM testings, contact angle measurements, and delayed icing experiments were systematically performed to investigate the effect of scanning speed on surface hydrophobicity. The results show that the high quality and uniform graphene can be achieved using the laser scanning speed of 125 mm/s. The periodic linear array structures can obviously increase the contact angle and suppress delayed icing. Furthermore, these structures have the enhanced ability of the electric heating deicing, which can reach 100°C and 240°C within 15 s and within 60 s under the DC voltage power supply ranging from 3 to 7 V, respectively. These results indicate that the LIG technique can be developed to provide an efficient, economical, and convenient approach for preparing graphene and the hydrophobic surface array structure based on LIG has considerable potential for deicing and anti-icing applications.