In this study, the effect of rhenium addition (2, 4, and 6 wt pct) and building orientation (0 and 90 deg) on the microstructure and corrosion resistance of Inconel 718 (IN718) alloy processed by selective laser melting (SLM) was investigated. Microstructure characterization showed that the as-built IN718-Re alloys consist of columnar grains growing parallel to the building direction (Z-axis). Each columnar grain was characterized by a fine columnar/cellular dendritic substructure with Nb- and Mo-rich Laves phases and MC-type carbides embedded in the interdendritic spaces. Rhenium addition segregated to γ phase dendrites which resulted in an increase of the columnar/cellular substructures width with increasing Re content. Due to a strong microstructure anisotropy of SLM-processed IN718-Re alloys, the corrosion properties were examined for mutually perpendicular planes: XY (90 deg samples) and XZ (0 deg). The presence of rhenium enhanced the corrosion resistance of IN718 alloy in 0.1 M Na₂SO₄and NaCl solutions at both exposed planes. The corrosion current density was significantly reduced for IN718-Re alloys and increasing Re content correlated with a more positive shift in corrosion potential. Moreover, the XY plane possessed better corrosion resistance than the XZ plane due to the higher fraction of laser overlapping areas observed for the XZ plane.

For the first time, the three-dimensional (3D) internal structure of naturally produced Didymosphenia geminata frustules were nondestructively visualized at sub-100 nm resolution. The well-optimized hierarchical structures of these natural organisms provide insight that is needed to design novel, environmentally friendly functional materials. Diatoms, which are widely distributed in freshwater, seawater and wet soils, are well known for their intricate, siliceous cell walls called ‘frustules’. Each type of diatom has a specific morphology with various pores, ribs, minute spines, marginal ridges and elevations. In this paper, the visualization is performed using nondestructive nano X-ray computed tomography (nano-XCT). Arbitrary cross-sections through the frustules, which can be extracted from the nano-XCT 3D data set for each direction, are validated via the destructive focused ion beam (FIB) cross-sectioning of regions of interest (ROIs) and subsequent observation by scanning electron microscopy (SEM). These 3D data are essential for understanding the functionality and potential applications of diatom cells.

Synthesis and characterization of composite shear thickening fluids (STFs) containing carbon nanofillers are presented. Shear thickening fluids have attracted particular scientific and technological interest due to their unique ability to abruptly increase viscosity in the case of a sudden impact. The fluids have been developed as a potential component of products with high energy absorbing efficiency. This study reports on the rheological behavior, stability, and microstructure of the STFs modified with the following carbon nanofillers: multi-walled carbon nanotubes, reduced graphene oxide, graphene oxide, and carbon black. In the current experiment, the basic STF was made as a suspension of silica particles with a diameter of 500 nm in polypropylene glycol and with a molar mass of 2000 g/mol. The STF was modified with carbon nanofillers in the following proportions: 0.05, 0.15, and 0.25 vol.%. The addition of the carbon nanofillers modified the rheological behavior and impact absorption ability; for the STF containing 0.25 vol.% of carbon nanotubes, an increase of force absorption up to 12% was observed.