An integrated magnetic nanosensor based on a niobium dc SQUID (superconducting quantum interference device) for nanoscale applications is presented. The sensor, having a washer shape with a hole of 200 nm and two Josephson-Dayem nanobridges of 80 nm × 100 nm, consists of a Nb(30 nm)/Al(30 nm) bilayer patterned by electron beam lithography (EBL) and shaped by lift-off and reactive ion etch (RIE) processes. The presence of the niobium coils, integrated on-chip and tightly coupled to the SQUID, allows us to easily excite the sensor in order to get the voltage-flux characteristics and to flux bias the SQUID at its optimal point. The measurements were performed at liquid helium temperature. A voltage swing of 75 µV and a maximum voltage-flux transfer coefficient (responsivity) as high as 1 mV/Φ(0) were directly measured from the voltage-flux characteristic. The noise measurements were performed in open loop mode, biasing the SQUID with a dc magnetic flux at its maximum responsivity point and using direct-coupled low-noise readout electronics. A white magnetic flux noise spectral density as low as 2.5 μΦ(0) Hz(-1/2) was achieved, corresponding to a magnetization or spin sensitivity in units of the Bohr magneton of 100 spin Hz(-1/2). Possible applications of this nanosensor can be envisaged in magnetic detection of nanoparticles and small clusters of atoms and molecules, in the measurement of nanoobject magnetization, and in quantum computing.
A high sensitive nano superconducting quantum interference device (nanoSQUID) operating as a magnetic flux to critical current transducer with a suitable feedback circuit is employed to measure the magnetization of ferrimagnetic iron oxide nanoparticles. An improved SQUID responsivity has been obtained by using a loop inductance asymmetry. Iron oxide nanoparticles having a mean diameter of 8 nm have been excited by applying a polarizing field in the plane of the nanoSQUID loop. The field dependence of the nanoparticle magnetization at T = 4.2 K shows magnetic hysteresis. Magnetic relaxation measurements are reported and compared with those obtained by using a commercial measurement system.
We present an ultra high sensitive three-dimensional nano Superconducting QUantum Interference Device (nanoSQUID) fabricated by using the Focused Ion Beam sculpting technique. Based on a fully niobium technology, the nanodevice consists in a niobium superconducting loop (0.2 μm2) interrupted by two nanometric Nb/Al-AlOx/Nb Josephson junctions. The nanoSQUID exhibited an intrinsic magnetic flux noise as low as 0.65 μΦ0/Hz1/2 corresponding to a spin noise less than 10 Bohr magnetons per unit of bandwidth. It has been successfully employed in nanoparticle magnetic relaxation measurements. Due to its excellent performance, reliability, and robustness, we believe that the proposed nanoSQUID offers a crucial step toward a wide employment of nanoSQUIDs in the nanoscience.