Ru/B4C multilayer mirrors are used for hard X-ray monochromators with moderate spectral resolution and high integral flux. To overcome the problem of large compressive stress inherent in Ru/B4C multilayers, a reactive sputtering technique using a mixture working gas of argon and nitrogen with different partial pressures was tested, and the fabricated multilayers had a period of 3 nm. The intrinsic stress was essentially reduced after nitridation and relaxed to zero value at approximately 15% partial pressure of nitrogen in the working gas. Interface roughness was slightly increased which can be caused by the polycrystalline structure inside the nitridated samples. More importantly, the nitridated multilayers showed an enhanced reflectance (67% at 8.04 keV photon energy) as compared with the one fabricated with pure Ar (54%). The structure analysis with transmission electron microscopy and X-ray photoelectron spectroscopy demonstrated that nitrogen incorporated into a multilayer structure was mostly located in the B4C layers forming BN compounds, which suppressed the diffusion of boron, stabilized the interfaces and enhanced the reflectance.
Surface wrinkling method is used to fabricate a 1-dimensional nanostructure. The structure is transferred to an ultraviolet cured polymer which is used as an alignment layer. The anisotropic geometry serves as a guide for aligning liquid crystal molecules uniformly without defects. The TN-LC cell showed a successful LC switching, with a response time of 20.5 ms, and a threshold voltage of 2.00 V. It also exhibited high thermal stability above 180°C. The proposed UV-cured polymers with 1-D nano wrinkle geometry can be a candidate for alternative alignment techniques, for advanced liquid crystal devices with high thermal budgets.
Process optimisation for increasing the response speed of optical driving liquid crystal cell was investigated in this paper. It is demonstrated that by filling LC in atmosphere condition rewriting time could be decreased to 6 s with good repeatability. Increasing the spin coating speed, the rewriting time could also decrease the azimuthal anchoring energy, but it will cause non-continuous film form of alignment layer, which causes large speed dispersion that is not good for practical use. Serial experiments show that with smaller azimuthal anchoring energy the rewriting time could be smaller. The results demonstrate that with proper fabrication process of alignment layer for liquid crystal optical rewritable e-paper, azimuthal anchoring energy could be adjusted to an optimal value, which is beneficial for achieving fastest rewriting speed and at the same time strong enough to well align LC. GRAPHICAL ABSTRACT
It is very difficult to display greyscale for an optically driving liquid crystal display (ODLCD) because the driving unit and display unit are separate, and there are no electronics in the display part of ODLCD. In this paper, two greyscale generation methods are proposed to achieve this goal. Six and nine grey levels are separately achieved through the two methods. Graphical Abstract